4-甲基-2-苯基-喹啉合成路线 （共 49 条）
反应条件
1: aq. H2SO4
2: DDQ / benzene
View Scheme
参考文献
Kouznetsov; Urbina; Palma; Lopez; Devia; Enriz; Zacchino
Molecules, 2000 , vol. 5, # 3 p. 428 - 430
反应条件
zinc(II) chloride in toluene
T=160°C; 0.5 h; Microwave irradiationIonic liquid;
参考文献
Portela-Cubillo, Fernando; Scott, Jackie S.; Walton, John C.
Journal of Organic Chemistry, 2009 , vol. 74, # 14 p. 4934 - 4942
反应条件
tetrabutylammomium bromide; palladium diacetate; sodium carbonate in N,N-dimethyl-formamide
T=60°C; Heck Reaction; 18 h; Catalytic behavior; Solvent; regioselective reaction;
参考文献
Martinez-Estibalez, Unai; Garcia-Calvo, Oihane; Ortiz-De-Elguea, Veronica; Sotomayor, Nuria; Lete, Esther
European Journal of Organic Chemistry, 2013 , # 15 p. 3013 - 3022
反应条件
in diethyl ether; pentane
参考文献
Greenhill; Loghmani-Khouzani; Maitland
Canadian Journal of Chemistry, 1991 , vol. 69, # 4 p. 696 - 701
反应条件
1: 28 percent / InCl3 / acetonitrile / 0.05 h / Heating; microwave irradiation
View Scheme
参考文献
Duvelleroy, Dorothee; Perrio, Cecile; Parisel, Olivier; Lasne, Marie-Claire
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3794 - 3804
反应条件
1: 28 percent / InCl3 / acetonitrile / 0.05 h / Heating; microwave irradiation
View Scheme
参考文献
Duvelleroy, Dorothee; Perrio, Cecile; Parisel, Olivier; Lasne, Marie-Claire
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3794 - 3804
反应条件
1.1: diethyl ether / 18 h / |Molecular sieve; |Reflux
2.1: tetrahydrofuran / -78 - -42 °C / |Inert atmosphere
2.2: -42 °C / |Inert atmosphere
3.1: palladium diacetate; sodium carbonate; tetrabutylammomium bromide / N,N-dimethyl-formamide / 18 h / 60 °C
View Scheme
参考文献
Martinez-Estibalez, Unai; Garcia-Calvo, Oihane; Ortiz-De-Elguea, Veronica; Sotomayor, Nuria; Lete, Esther
European Journal of Organic Chemistry, 2013 , # 15 p. 3013 - 3022
反应条件
1.1: tetrahydrofuran / -78 - -42 °C / |Inert atmosphere
1.2: -42 °C / |Inert atmosphere
2.1: palladium diacetate; sodium carbonate; tetrabutylammomium bromide / N,N-dimethyl-formamide / 18 h / 60 °C
View Scheme
参考文献
Martinez-Estibalez, Unai; Garcia-Calvo, Oihane; Ortiz-De-Elguea, Veronica; Sotomayor, Nuria; Lete, Esther
European Journal of Organic Chemistry, 2013 , # 15 p. 3013 - 3022
反应条件
1: Mg / diethyl ether / 10 °C
2: aq. H2SO4
3: DDQ / benzene
View Scheme
参考文献
Kouznetsov; Urbina; Palma; Lopez; Devia; Enriz; Zacchino
Molecules, 2000 , vol. 5, # 3 p. 428 - 430
反应条件
1: 94 percent / triethylamine / tetrahydrofuran / 3 h / 0 °C
2: 80 percent / Na2HPO4 / CH2Cl2 / 0 °C
3: 92 percent / diphenyl ether / 43 h / Irradiation
View Scheme
参考文献
Qiang, Lin Guo; Baine, Neil H.
Tetrahedron Letters, 1988 , vol. 29, # 29 p. 3517 - 3520
