4-甲基-2-苯基-喹啉合成路线 （共 49 条）
反应条件
1: in tetrahydrofuran; diethyl ether; cyclohexane
T=-30°C; Addition; 1 h;
2: in tetrahydrofuran; pentane
T=-30 - 25°C; Oxidation; 1 h;
参考文献
Tagawa, Yoshinobu; Nomura, Manami; Yamashita, Hiroyuki; Goto, Yoshinobu; Hamana, Masatomo
Heterocycles, 1999 , vol. 51, # 10 p. 2385 - 2397
反应条件
benzophenone; cis-[RuCl2(dimethylsulfoxide-S)3(dimethylsulfoxide-O)]; potassium tert-butylate
T=100°C; indirect Friedlaender annulation; 48 h;
参考文献
Martinez, Ricardo; Ramon, Diego J.; Yus, Miguel
European Journal of Organic Chemistry, 2007 , # 10 p. 1599 - 1605
反应条件
urea in toluene
T=150°C; 48 h;
参考文献
Qi, Chuanmei; Zheng, Qingwei; Hua, Ruimao
Tetrahedron, 2009 , vol. 65, # 7 p. 1316 - 1320
反应条件
2,2,2-trimethylacetic acid; silver nitrate in acetonitrile
参考文献
Minisci, Francesco; Vismara, Elena; Romano, Ugo
Tetrahedron Letters, 1985 , vol. 26, # 39 p. 4803 - 4806
反应条件
in diphenylether
43 h; Irradiation;
参考文献
Qiang, Lin Guo; Baine, Neil H.
Tetrahedron Letters, 1988 , vol. 29, # 29 p. 3517 - 3520
反应条件
1.1: n-BuLi / tetrahydrofuran / 0.5 h / 0 °C
1.2: 72 percent / tetrahydrofuran / 1 h / 0 °C
2.1: 82 percent / Fe; aq. HCl / ethanol / 2 h / 80 °C
View Scheme
参考文献
Sandelier, Matthew J.; DeShong, Philip
Organic Letters, 2007 , vol. 9, # 17 p. 3209 - 3212
反应条件
1: Na2SO4 / benzene / Heating
2: 25.3 percent / BF3*Et2O / benzene / 48 h / Heating
View Scheme
参考文献
Kametani, Tetsuji; Takeda, Hajime; Suzuki, Yukio; Kasai, Hiroko (nee Furuyama); Honda, Toshio
Heterocycles, 1986 , vol. 24, # 12 p. 3385 - 3395
反应条件
boron trifluoride diethyl etherate in dichloromethane
2 h; Heating;
参考文献
Kouznetsov, Vladimir V.; Melendez Gomez, Carlos M.; Urbina Gonzalez, Juan M.; Stashenko, Elena E.; Bahsas, Ali; Amaro-Luis, Juan
Journal of Heterocyclic Chemistry, 2007 , vol. 44, # 3 p. 551 - 555
参考文献
Goldberg; Levine
Journal of the American Chemical Society, 1955 , vol. 77, p. 3647
Full Text View citing articles Show Details
Tarbell et al.
Journal of the American Chemical Society, 1945 , vol. 67, p. 1582
反应条件
1.1: POCl3; Et3N / tetrahydrofuran / 0 °C
2.1: BuLi / tetrahydrofuran; hexane / 0.25 h / 0 °C
2.2: 70 percent / tetrahydrofuran; hexane / 20 °C
3.1: 55 percent / 1,2-dimethoxy-ethane; hexane / -78 - 20 °C
View Scheme
参考文献
Kobayashi, Kazuhiro; Yoneda, Keiichi; Miyamoto, Kazuna; Morikawa, Osamu; Konishi, Hisatoshi
Tetrahedron, 2004 , vol. 60, # 50 p. 11639 - 11645
