2,4,6-三甲基溴化苄合成路线 （共 15 条）
反应条件
in ethanol; water 4 h; Heating;
参考文献
Law, Ho; Dukat, Malgorzata; Teitler, Milt; Lee, David K. H.; Mazzocco, Lucia; Kamboj, Raj; Rampersad, Vik; Prisinzano, Thomas; Glennon, Richard A.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 13 p. 2243 - 2251
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; iron(II) oxalate dihydrate T=155 - 160°C; 0.166667 h;
参考文献
Khurana, Jitender M.; Chauhan, Sushma; Maikap, Golak C.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 10 p. 1737 - 1740
参考文献
Carre
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1910 , vol. 151, p. 150
Bulletin de la Societe Chimique de France, 1910 , vol. <4> 7, p. 842
反应条件
sodium periodate in N,N-dimethyl-formamide T=150°C; 0.833333 h;
参考文献
Hullio, Ahmed Ali; Mastoi; Khan, Khalid
Asian Journal of Chemistry, 2011 , vol. 23, # 12 p. 5411 - 5418
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; iron(II) oxalate dihydrate T=155 - 160°C; 0.166667 h;
参考文献
Khurana, Jitender M.; Chauhan, Sushma; Maikap, Golak C.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 10 p. 1737 - 1740
反应条件
phosphorus tribromide in tetrahydrofuran
T=0°C; Inert atmosphere;
参考文献
Tsoi, Yuk-Tai; Zhou, Zhongyuan; Yu, Wing-Yiu
Organic Letters, 2011 , vol. 13, # 19 p. 5370 - 5373
反应条件
hydrogen bromide; acetic acid
T=40 - 50°C; 2 h;
参考文献
Made, A. W. van der; Made, R. H. van der
Journal of Organic Chemistry, 1993 , vol. 58, # 5 p. 1262 - 1263
反应条件
hydrogen bromide; tetradecyltrimethylammonium bromide in water
T=80 - 90°C; Substitution; 8 h;
参考文献
Mitchell, Reginald H.; Zhang, Limin
Journal of Organic Chemistry, 1999 , vol. 64, # 19 p. 7140 - 7152
反应条件
1: LiAlH4; diethyl ether
2: aqueous hydrobromic acid
View Scheme
参考文献
Hauser; Van Eenam
Journal of the American Chemical Society, 1957 , vol. 79, p. 5512,5518
反应条件
hydrogen bromide; acetic acid
T=100°C;
参考文献
Carre
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1910 , vol. 151, p. 150
Bulletin de la Societe Chimique de France, 1910 , vol. <4> 7, p. 842
