1,4-环己二酮单乙二醇缩酮合成路线 （共 270 条）
反应条件
formaldehyd; silica gel; iron(III) chloride T=20°C; 0.416667 h;
参考文献
Fadel, Antoine; Yefsah, Ramdane; Salauen, Jacques
Synthesis, 1987 , # 1 p. 37 - 40
反应条件
in water; dimethyl sulfoxide T=150°C; 8 h;
参考文献
Kametani, Tetsuji; Kondoh, Hirotsune; Honda, Toshio; Ishizone, Hiroyuki; Suzuki, Yukio; Mori, Wakako
Chemistry Letters, 1989 , p. 901 - 904
反应条件
acetic acid in dichloromethane T=20°C; 30 h;
参考文献
Crombie, Leslie; Crombie, W. Mary L.; Jamieson, Sally V.; Tuchinda Patoomratana; Whitaker, Alison J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1485 - 1492
参考文献
Gardner et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 1206,1209
Full Text Show Details
Leonard et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 1482,1484
反应条件
1: benzene; toluene-4-sulfonic acid / Entfernen des entstehenden Wassers 2: sodium; xylene View Scheme
参考文献
Leonard et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 1482,1484
反应条件
toluene-4-sulfonic acid in benzene Heating;
参考文献
Crombie, Leslie; Crombie, W. Mary L.; Jamieson, Sally V.; Tuchinda Patoomratana; Whitaker, Alison J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 1485 - 1492
反应条件
1.1: Et3N / diethyl ether / 7 h / 20 °C 2.1: Co2(CO)8; Et3N / diethyl ether / 0.25 h / 20 °C 2.2: 74 percent / H2O / methanol / 0.5 h / 20 °C View Scheme
参考文献
Mukai, Chisato; Nomura, Izumi; Kataoka, Osamu; Hanaoka, Miyoji
Synthesis, 1999 , # 11 p. 1872 - 1874
反应条件
1: 62 percent / NaH / dimethylformamide / 25 - 60 °C 2: 83 percent / NaHCO3 / dioxane; H2O / Irradiation View Scheme
参考文献
Ogura, Katsuyuki; Ohtsuki, Kazuo; Nakamura, Masami; Yahata, Nobuhiro; Takahashi, Kazumasa; Iida, Hirotada
Tetrahedron Letters, 1985 , vol. 26, # 20 p. 2455 - 2458
参考文献
Gardner et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 1206,1209
反应条件
1: benzene; toluene-4-sulfonic acid / Erwaermen des Reaktionsprodukts mit methanol. Natronlauge 2: chromium (VI)-oxide; pyridine View Scheme
参考文献
Prins
Helvetica Chimica Acta, 1957 , vol. 40, p. 1621,1625
