2-苯基-4-五亚乙基六胺-2-醇合成路线 （共 59 条）
反应条件
tin(ll) chloride in acetonitrile 1 h;
参考文献
Yasuda, Makoto; Sugawa, Yoshihiro; Yamamoto, Akihiro; Shibata, Ikuya; Baba, Akio
Tetrahedron Letters, 1996 , vol. 37, # 33 p. 5951 - 5954
反应条件
1: in tetrahydrofuran T=-78°C; 3 h; 2: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran Heating;
参考文献
Canales, Eda; Prasad, K. Ganeshwar; Soderquist, John A.
Journal of the American Chemical Society, 2005 , vol. 127, # 33 p. 11572 - 11573
反应条件
in diethyl ether T=20°C; 0.5 h;
参考文献
Shen, Kao-Hsien; Yao, Ching-Fa
Journal of Organic Chemistry, 2006 , vol. 71, # 10 p. 3980 - 3983
反应条件
diiodosamarium in various solvent(s) T=0°C; 2 h;
参考文献
Hamann-Gaudinet, Beatrice; Namy, Jean-Louis; Kagan, Henri B.
Tetrahedron Letters, 1997 , vol. 38, # 37 p. 6585 - 6588
反应条件
in Petroleum ether T=65°C; 4 h;
参考文献
Boudin, Alain; Cerveau, Genevieve; Chuit, Claude; Corriu, Robert J.P.; Reye, Catherine
Tetrahedron, 1989 , vol. 45, # 1 p. 171 - 180
反应条件
1: isopropenylbenzene With oxygen in dichloromethane T=-78°C; ozonolysis; 0.166667 h; 2: allyl bromide With ammonium chloride; zinc in tetrahydrofuran T=0°C; Rearrangement; 0.25 h;
参考文献
Schloss, Jeffrey D.; Paquette, Leo A.
Synthetic Communications, 1998 , vol. 28, # 15 p. 2887 - 2892
反应条件
tetrakis(triphenylphosphine) palladium(0); diethylzinc in tetrahydrofuran; hexane 6 h; Ambient temperature;
参考文献
Yasui, Kengo; Goto, Youichi; Yajima, Takafumi; Taniseki, Yasue; Fugami, Keigo; Tanaka, Akihiro; Tamaru, Yoshinao
Tetrahedron Letters, 1993 , vol. 34, # 47 p. 7619 - 7622
反应条件
cerium; 3-iodoprop-1-ene; iodine in tetrahydrofuran T=-20°C; 3 h; var. reag.: Me-, Et-, PhI;
参考文献
Fukuzawa, Shin-ichi; Fujinami, Tatsuo; Sakai, Shizuyoshi
Journal of Organometallic Chemistry, 1986 , vol. 299, p. 179 - 186
反应条件
AlCl3 etherate in tetrahydrofuran T=-78°C; 1 h; synthesis of allylic alcohols; other ketones, other pentaorganylstiboranes;
参考文献
Zhang, Li-Jun; Huang, Yao-Zeng; Jiang, Hong-Xia; Duan-Mu, Jun; Liao, Yi
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 774 - 777
反应条件
vanadium(III) chloride; benzaldehyde in diethyl ether; dichloromethane 14 h; -70 to 20 deg C in 14 h;
参考文献
Kauffmann, Thomas; Bonrath, Werner; Beirich, Christoph; Li, Weichang; Pahde, Claudia; et al.
Chemische Berichte, 1993 , vol. 126, # 9 p. 2093 - 2100
