联苯-4,4-草酸二乙酯合成路线 （共 84 条）
反应条件
1: With zinc in tetrahydrofuran Heating; 2: With (3,5-dinitrophenyl)(4-methylpiperazin-1-yl)methanone; copper(I) bromide dimethylsulfide complex in N,N-dimethyl acetamide T=22°C; 1 h;
参考文献
Moncomble, Aurelien; Floch, Pascal Le; Gosmini, Corinne
Chemistry - A European Journal, 2009 , vol. 15, # 19 p. 4770 - 4774
反应条件
PEG 4000; palladium diacetate; potassium carbonate T=120°C; 4 h;
参考文献
Wang, Liang; Zhang, Yuhong; Liu, Leifang; Wang, Yanguang
Journal of Organic Chemistry, 2006 , vol. 71, # 3 p. 1284 - 1287
反应条件
p-benozquinone; (SIPr)Pd(OAc)2(H2O) in methanol T=20°C; 24 h;
参考文献
Yamamoto, Yoshihiko
Synlett, 2007 , # 12 p. 1913 - 1916
反应条件
bromobenzene; zinc dibromide; zinc; acetic acid; cobalt(II) dibromide in acetonitrile T=20°C; 3 h;
参考文献
Perichon, Jacques; Gosmini, Corinne; Bastienne, Mylene; Gomes, Paulo
Patent: US2004/186328 A1, 2004 ;
Location in patent: Page 12 ;
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; [(Ph2CH=NOH)PdCl]2 in benzene T=120°C; 3 h;
参考文献
Ramesh, Chinnasamy; Nakamura, Ryo; Kubota, Yoshihiro; Miwa, Minoru; Sugi, Yoshihiro
Synthesis, 2003 , # 4 p. 501 - 504
反应条件
1: ethylene,methyl acetate With indium(III) chloride; dimethyl(n-butyl)amine; lithium chloride; indium; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=35°C; 2: 4-iodobenzoic acid ethyl ester in N,N-dimethyl-formamide T=100°C;
参考文献
Seomoon, Dong; Lee, Kooyeon; Kim, Hyunseok; Lee, Phil Ho
Chemistry - A European Journal, 2007 , vol. 13, # 18 p. 5197 - 5206
反应条件
copper(l) iodide; bis(η3-allyl-μ-chloropalladium(II)); [-MeSi(H)O-]3-5; potassium fluoride in N,N-dimethyl-formamide T=20°C; 2 h;
参考文献
Denmark, Scott E.; Kobayashi, Tetsuya
Journal of Organic Chemistry, 2003 , vol. 68, # 13 p. 5153 - 5159
反应条件
1: With [resin-CH2N(CH3)3]2CO3; Pd(PAnPh2)2Cl2 in water; N,N-dimethyl-formamide T=80°C; Suzuki coupling; 16 h; 2: With maleimido-CH2-PS resin in water; N,N-dimethyl-formamide T=90°C; 10 h;
参考文献
Lan, Ping; Berta, Daniela; Porco Jr., John A.; South, Michael S.; Parlow, John J.
Journal of Organic Chemistry, 2003 , vol. 68, # 25 p. 9678 - 9686
反应条件
1: With [resin-CH2N(CH3)3]2CO3; Pd(PAnPh2)2Cl2 in water; N,N-dimethyl-formamide T=80°C; Suzuki coupling; 16 h; 2: With maleimido-CH2-PS resin in water; N,N-dimethyl-formamide T=90°C; 10 h;
参考文献
Lan, Ping; Berta, Daniela; Porco Jr., John A.; South, Michael S.; Parlow, John J.
Journal of Organic Chemistry, 2003 , vol. 68, # 25 p. 9678 - 9686
反应条件
1: Methallyl acetate With indium(III) chloride; dimethyl(n-butyl)amine; lithium chloride; indium; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=35°C; 2: 4-iodobenzoic acid ethyl ester in N,N-dimethyl-formamide T=100°C;
参考文献
Seomoon, Dong; Lee, Kooyeon; Kim, Hyunseok; Lee, Phil Ho
Chemistry - A European Journal, 2007 , vol. 13, # 18 p. 5197 - 5206
