2,4-二甲基萘-1-醇合成路线 （共 18 条）
反应条件
in tetrahydrofuran T=25°C; ΔH; Thermodynamic data;
参考文献
Journal of the American Chemical Society, , vol. 114, # 23 p. 9209 - 9210
反应条件
oxygen in chloroform P=760 Torr; 17 h; Ambient temperature;
参考文献
Greenland, Harry; Pinhey, John T.; Sternhell, Sever
Australian Journal of Chemistry, 1987 , vol. 40, # 2 p. 325 - 331
反应条件
copper(II) bis(trifluoromethanesulfonate) in 1,2-dichloro-ethane
T=20°C; 0.3 h; Inert atmosphere;
参考文献
Peng, Fangzhi; Fan, Baomin; Shao, Zhihui; Pu, Xuewei; Li, Penghui; Zhang, Hongbin
Synthesis, 2008 , # 19 art. no. F11408SS, p. 3043 - 3046
反应条件
copper(II) bis(trifluoromethanesulfonate) in dichloromethane
T=20°C; 1.5 h;
参考文献
Sawama, Yoshinari; Kawamoto, Koichi; Satake, Hiroyuki; Krause, Norbert; Kita, Yasuyuki
Synlett, 2010 , # 14 art. no. U03810ST, p. 2151 - 2155
反应条件
palladium diacetate; caesium carbonate; triphenylphosphine in N,N-dimethyl-formamide; toluene
T=120°C; Condensation; cyclization; decarbonylation; 2 h;
参考文献
Terao, Yoshito; Satoh, Tetsuya; Miura, Masahiro; Nomura, Masakatsu
Tetrahedron, 2000 , vol. 56, # 10 p. 1315 - 1320
反应条件
anhydrous iron chloride; trimethylsilylazide in chloroform
T=-40 - 0°C; 8 h; Inert atmosphere;
参考文献
Sawama, Yoshinari; Ogata, Yuta; Kawamoto, Koichi; Satake, Hiroyuki; Shibata, Kyoshiro; Monguchi, Yasunari; Sajiki, Hironao; Kita, Yasuyuki
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 2-3 p. 517 - 528
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=0°C; 2 h; Inert atmosphere;
参考文献
Sawama, Yoshinari; Kawamoto, Koichi; Satake, Hiroyuki; Krause, Norbert; Kita, Yasuyuki
Synlett, 2010 , # 14 art. no. U03810ST, p. 2151 - 2155
反应条件
aluminum oxide
T=300°C;
参考文献
Klemm,L.H. et al.
Journal of Organic Chemistry, 1968 , vol. 33, p. 1480 - 1488
反应条件
monohydrate copper acetate; diphenyl-N,N-bis-((S,S)-1-phenyl-ethyl)phosphinamine in hexane; tert-butyl methyl ether
T=20°C; 20.05 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Millet, Renauds; Gremaud, Ludovic; Bernardez, Tania; Palais, Laetitia; Alexakis, Alexandre
Synthesis, 2009 , # 12 art. no. C01409SS, p. 2101 - 2112
反应条件
in acetonitrile
T=25°C; 0.0833333 h; UV-irradiation;
参考文献
Mori, Tadashi; Takamoto, Makoto; Saito, Hideaki; Furo, Takahiro; Wada, Takehiko; Inoue, Yoshihisa
Chemistry Letters, 2004 , vol. 33, # 3 p. 256 - 257
