反应条件
in diethyl ether GaCl3 was dissolved in diethyl ether, stirred soln. was cooled in an ice bath, addn. of the silane, the soln. was refluxed for 7 h, pptn., all steps under N2 or Ar; the liquid portion was removed from the solid by vacuum distn., the solid was recrystd. (CH2Cl2), elem. anal.;
参考文献
Inorganic Chemistry, , vol. 30, p. 4136 - 4140
