1,1'-氧基二(环己烷)合成路线 (共 57 条)
反应条件
Fe-montmorillonite (Fe-Mn) (solid acid) in dichloromethane
0.5 h; Ambient temperatureother ketones, aldehydes and esters; other hydrosilanes; var. solid acids and bases; trifluoromethanesulfonic acid and its salt; Product distributionMechanism;
参考文献
Onaka, Makoto; Higuchi, Katsumi; Nanami, Hiroyuki; Izumi, Yusuke
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 9 p. 2638 - 2645
反应条件
sodium hydroxide; sodium tetrahydroborate; Hg(NO3)2
1.) 60 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Brown, Herbert C.; Kurek, Joseph T.; Rei, Min-Hon; Thompson, Kerry L.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2551 - 2557
反应条件
MoVIO2(acetylacetone)2; diphenylether; toluene-4-sulfonic acid in toluene
T=100°C; 10 h; Product distribution;
参考文献
Lorber, Christian Y.; Pauls, Irene; Osborn, John A.
Bulletin de la Societe Chimique de France, 1996 , vol. 133, # 7-8 p. 755 - 758
反应条件
copper acetylacetonate; carbon tetrabromide
T=150°C; 4 h;
参考文献
Khusnutdinov, R. I.; Bayguzina, A. R.; Gimaletdinova, L. I.; Dzhemilev, U. M.
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 9 p. 1191 - 1196,6
Zhurnal Organicheskoi Khimii, 2012 , vol. 48, # 9 p. 1191 - 1196,6
参考文献
Fichter; Siegrist
Helvetica Chimica Acta, 1932 , vol. 15, p. 698,702
反应条件
in cyclohexane
Irradiation;
参考文献
Gilbert, Andrew; Taylor, Grahame N.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1761 - 1768
反应条件
hydrogen; Rh/Al2O3
P=760 Torr; Ambient temperaturesolid substrate; solid catalyst; various metal salts of substrate; various conversion rates; various product distributions; various reaction times; other catalysts; catalyst particles coated by teflon; Product distributionMechanism;
参考文献
Lamartine, Roger; Perrin, Robert; Thozet, Alain; Perrin, Monique
Molecular Crystals and Liquid Crystals (1969-1991), 1983 , vol. 96, p. 57 - 70
反应条件
in cyclohexane
Irradiation;
参考文献
Gilbert, Andrew; Taylor, Grahame N.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1761 - 1768
参考文献
Criegee; Vogel; Hoeger
Chemische Berichte, 1952 , vol. 85, p. 144,145
反应条件
pentacarbonyliron(0); 1-chloro-3,3,3-trichloropropane
further reagents; Product distribution;
参考文献
Chukovskaya, E. Ts.; Rozhkova, M. A.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 7 p. 1406 - 1409
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 7 p. 1582 - 1585