3,3-二甲基-2-丁醇合成路线 （共 125 条）
反应条件
pyridine-nonakis(hydrogen fluoride); hydrogen fluoride in n-heptane 4 h; Ambient temperature;
参考文献
Brower, K. R.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 798 - 802
反应条件
[(C4Ph4COHOCC4Ph4)(μ-H)][(CO)4Ru2]; Novozym(R) 435; 2,4-dimethylpentan-3-one in toluene T=70°C; P=157.513 Torr; 40 h;
参考文献
Verzijl, Gerard K.M.; De Vries, Johannes G.; Broxterman, Quirinus B.
Tetrahedron Asymmetry, 2005 , vol. 16, # 9 p. 1603 - 1610
反应条件
palladium diacetate; oxygen; (-)-sparteine in 1,2-dichloro-ethane T=80°C; Title compound not separated from byproducts.;
参考文献
Xu, Daqian; Wang, Shoufeng; Shen, Zhiqiang; Xia, Chungu; Sun, Wei
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 14 p. 2730 - 2732
反应条件
lipase from Pseudomonas cepacia immobilized on ceramic in toluene T=40°C; 24 h; Title compound not separated from byproducts;
参考文献
Ghanem, Ashraf; Schurig, Volker
Tetrahedron Asymmetry, 2003 , vol. 14, # 17 p. 2547 - 2555
反应条件
[bis(acetoxy)iodo]benzene; potassium bromide in dichloromethane; water T=20°C; 1 h;
参考文献
Sun, Wei; Wu, Xiaomei; Xia, Chungu
Helvetica Chimica Acta, 2007 , vol. 90, # 3 p. 623 - 626
反应条件
3 A molecular sieve; Humicola insolens ferulic acid esterase T=45°C; 576 h;
参考文献
Hatzakis, Nikos S.; Smonou, Ioulia
Bioorganic Chemistry, 2005 , vol. 33, # 4 p. 325 - 337
反应条件
enantiomeric resolution by complexation gas chromatography on nickel(II)bis<(1R)-3-(heptafluorobutyryl)camphorate> in squalane at 70 deg C;
参考文献
Schurig,V.; Buerkle,W.
Journal of the American Chemical Society, 1982 , vol. 104, p. 7573
反应条件
3 A molecular sieve; oxygen; (-)-sparteine; Pd((-)-sparteine)2Cl2 in tert-butyl alcohol
T=65°C; 20 h;
参考文献
Mandal, Sunil K.; Jensen, David R.; Pugsley, Jacob S.; Sigman, Matthew S.
Journal of Organic Chemistry, 2003 , vol. 68, # 11 p. 4600 - 4603
反应条件
[(C4Ph4COHOCC4Ph4)(μ-H)][(CO)4Ru2]; Novozym(R) 435; 2,4-dimethylpentan-3-one in toluene
T=70°C; P=157.513 Torr; 40 h;
参考文献
Verzijl, Gerard K.M.; De Vries, Johannes G.; Broxterman, Quirinus B.
Tetrahedron Asymmetry, 2005 , vol. 16, # 9 p. 1603 - 1610
反应条件
palladium diacetate; oxygen; (-)-sparteine in 1,2-dichloro-ethane
T=80°C; Title compound not separated from byproducts.;
参考文献
Xu, Daqian; Wang, Shoufeng; Shen, Zhiqiang; Xia, Chungu; Sun, Wei
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 14 p. 2730 - 2732
