in tetrahydrofuran; diethyl ether
T=-10 - 20°C; 2 h;
参考文献
Barluenga, Jose; Rubiera, Covadonga; Fernandez, Jose R.; Florez, Josefa; Yus, Miguel
Journal of Chemical Research, Miniprint, 1987 , # 12 p. 3242 - 3264
in acetonitrile
Electrolysis; under Ar, 1 equiv of 4-chlorobutyryl chloride; solvent contained 0.1 M Bu4NPF6, cathode was mercury pool, the anode a Pt grid; the electrolyses were carried at -1.1 V vs. SCE and stopped when the Faradaic current became negligible; the catholyte was diluted with water and the electrolysis products were extracted with diethyl ether; the crude product was subjected to column chromy. using as eluant 5/5 diethyl ether/hexane mixture; elem. anal.;
参考文献
Degrand, C; Gasquez, F.; Compagnon, P. L.
Journal of Organometallic Chemistry, 1985 , vol. 280, p. 87 - 94
