in cyclohexane
(N2 or Ar); a mixture of Pt-complex and P(C2H5)3 in cyclohexane heated at 157°C for 1.6-2.25 h; cooled to -196°C; warmed to 25°C; evapd.; dissolved in acetonitrile; separated; evapd.; dissolved in ether; methanol added; cooled to -78°C; concentrated; pptd.; recrystd. from methanol/ether; elem. anal.;
参考文献
Foley, Paul; DiCosimo, Robert; Whitesides, George M.
Journal of the American Chemical Society, 1980 , vol. 102, # 22 p. 6713 - 6725