2-苯基-1,3-二苄基咪唑烷合成路线 （共 14 条）
反应条件
1: THF-d8 (tetrahydrofuran-d8) / 264 h / phosphate buffer in D2O 2: THF-d8 (tetrahydrofuran-d8) / 240 h / phosphate buffer in D2O View Scheme
参考文献
Buchsnee Levrand, Barbara; Godin, Guillaume; Trachsel, Alain; De Saint Laumer, Jean-Yves; Lehn, Jean-Marie; Herrmann, Andreas
European Journal of Organic Chemistry, 2011 , # 4 p. 681 - 695
反应条件
water T=20°C; pH=6.5 - 7.0; 49 h; Aqueous phosphate buffer; Reactivity;
参考文献
Buchsnee Levrand, Barbara; Godin, Guillaume; Trachsel, Alain; De Saint Laumer, Jean-Yves; Lehn, Jean-Marie; Herrmann, Andreas
European Journal of Organic Chemistry, 2011 , # 4 p. 681 - 695
反应条件
hydrogen; palladium on activated charcoal in ethanol
T=0°C; P=760 Torr; 20 h;
参考文献
Pallavicini, Marco; Valoti, Ermanno; Piccolo, Oreste
Journal of Chemical Research, Synopses, 1995 , # 11 p. 472 - 473
参考文献
FIRMENICH SA; UNIVERSITE LOUIS PASTEUR; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE
Patent: WO2008/93272 A2, 2008 ;
Location in patent: Page/Page column 29-30 ;
反应条件
hydrogen; palladium on activated charcoal in ethanol
T=0°C; P=760 Torr; 20 h;
参考文献
Pallavicini, Marco; Valoti, Ermanno; Piccolo, Oreste
Journal of Chemical Research, Synopses, 1995 , # 11 p. 472 - 473
反应条件
sodium carbonate in decalin
T=140 - 145°C; 17 h;
参考文献
Glinka, Ryszard; Mikiciuk-Olasik, Elzbieta; Kotelko, Barbara; Strzelczyk, Marek
Polish Journal of Chemistry, 1980 , vol. 54, # 2 p. 203 - 212
反应条件
hydrogenchloride in decalin
T=170 - 180°C; 17 h;
参考文献
Glinka, Ryszard; Mikiciuk-Olasik, Elzbieta; Kotelko, Barbara; Strzelczyk, Marek
Polish Journal of Chemistry, 1980 , vol. 54, # 2 p. 203 - 212
反应条件
1: sodium tetrahydroborate / methanol / 20 - 70 °C / Inert atmosphere
2: THF-d8 (tetrahydrofuran-d8) / 600 h / phosphate buffer in D2O
3: THF-d8 (tetrahydrofuran-d8) / 600 h / phosphate buffer in D2O
4: THF-d8 (tetrahydrofuran-d8) / 264 h / phosphate buffer in D2O
View Scheme
参考文献
Buchsnee Levrand, Barbara; Godin, Guillaume; Trachsel, Alain; De Saint Laumer, Jean-Yves; Lehn, Jean-Marie; Herrmann, Andreas
European Journal of Organic Chemistry, 2011 , # 4 p. 681 - 695
反应条件
in isopropyl alcohol
2 h; Heating;
参考文献
Glinka, Ryszard; Mikiciuk-Olasik, Elzbieta; Kotelko, Barbara; Strzelczyk, Marek
Polish Journal of Chemistry, 1980 , vol. 54, # 2 p. 203 - 212
反应条件
1: THF-d8 (tetrahydrofuran-d8) / 600 h / phosphate buffer in D2O
2: THF-d8 (tetrahydrofuran-d8) / 600 h / phosphate buffer in D2O
3: THF-d8 (tetrahydrofuran-d8) / 264 h / phosphate buffer in D2O
View Scheme
参考文献
Buchsnee Levrand, Barbara; Godin, Guillaume; Trachsel, Alain; De Saint Laumer, Jean-Yves; Lehn, Jean-Marie; Herrmann, Andreas
European Journal of Organic Chemistry, 2011 , # 4 p. 681 - 695
