4-羟基-3-甲氧基肉桂醛合成路线 （共 28 条）
反应条件
lithium tri-t-butoxyaluminum hydride; copper(l) iodide T=-78°C; 1 h;
参考文献
Duran, E.; Gorrichon, L.; Cazaux, L.; Tisnes, P.
Tetrahedron Letters, 1984 , vol. 25, # 26 p. 2755 - 2758
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in tetrahydrofuran T=20°C; 7 h;
参考文献
Ozanne, Aurelie; Pouysegu, Laurent; Depernet, Dominique; Francois, Bruno; Quideau, Stephane
Organic Letters, 2003 , vol. 5, # 16 p. 2903 - 2906
反应条件
potassium hydroxide in ethanol 12 h;
参考文献
Daubresse; Francesch; Mhamdi; Rolando
Synthesis, 1994 , # 4 p. 369 - 371
反应条件
potassium phosphate buffer; [3.3.1]nonane; Byssochlamus fulva V107 in water Oxidation; pH=7.0; 36 h;
参考文献
Furukawa, Hirotaka; Wieser, Marco; Morita, Hiroshi; Nagasawa, Toru
Bioscience, Biotechnology and Biochemistry, 1999 , vol. 63, # 6 p. 1141 - 1142
反应条件
1: 1.) aqueous potassium carbonate, 2.) 10percent aq. HCl / 1.) tris-<2-(2-methoxyethoxy)ethyl>amine / 1.) dichloromethane, room temperature, 12 h, 2.) dichloromethane, room temperature, 12 h 2: 81 percent / KOH / aq. ethanol / 12 h View Scheme
参考文献
Daubresse; Francesch; Mhamdi; Rolando
Synthesis, 1994 , # 4 p. 369 - 371
反应条件
acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane 2 h;
参考文献
Joshi, Bhupendra P.; Sharma, Anuj; Sinha, Arun K.
Tetrahedron, 2006 , vol. 62, # 11 p. 2590 - 2593
反应条件
water; HUSY (Si/Al=15) T=250°C; P=5250.53 Torr; 2 h; Inert atmosphere; Product distribution / selectivity;
参考文献
COUNCIL OF SCIENTIFIC AND INDUSTRIAL RESEARCH
Patent: US2012/302796 A1, 2012 ;
Location in patent: Page/Page column 6; 7 ;
反应条件
2: 71 percent / LiAl(OBu)3H / CuI / 1 h / -78 °C View Scheme
参考文献
Duran, E.; Gorrichon, L.; Cazaux, L.; Tisnes, P.
Tetrahedron Letters, 1984 , vol. 25, # 26 p. 2755 - 2758
反应条件
1: NaH / tetrahydrofuran / 1 h / Ambient temperature 2: 79 percent 3: 1) NaBH4, 2) aq. oxalic acid View Scheme
参考文献
WAYNE STATE UNIVERSITY; DUTTA, Aloke, K.
Patent: WO2014/85600 A1, 2014 ;
反应条件
sodium tetrahydroborate; oxalic acid Multistep reaction;
参考文献
Herbert; Kattah; Knagg
Tetrahedron, 1990 , vol. 46, # 20 p. 7119 - 7138
