2-溴-1-(2,5-二氯苯基)乙酮合成路线 （共 7 条）
反应条件
hydrogen bromide; dihydrogen peroxide in 1,4-dioxane; water 20 h; Heating;
参考文献
Tillu, Vasudha H.; Shinde, Popat D.; Bedekar, Ashutosh V.; Wakharkar, Radhika D.
Synthetic Communications, 2003 , vol. 33, # 8 p. 1399 - 1403
反应条件
copper(ll) bromide in chloroform; ethyl acetate 5 h; Reflux;
参考文献
Roman, Gheorghe; Vlahakis, Jason Z.; Vukomanovic, Dragic; Nakatsu, Kanji; Szarek, Walter A.
ChemMedChem, 2010 , vol. 5, # 9 p. 1541 - 1555
反应条件
in ethanol T=80°C; Hantzsch thiazole synthesis; 0.333333 h; Microwave irradiation;
参考文献
Gaikwad, Sudhakar A.; Patil, Amol A.; Deshmukh, Madhukar B.
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 1 p. 103 - 109
反应条件
ammonium chloride; zinc in ethanol T=80°C; 0.00833333 h; microwave irradiation;
参考文献
Li, Jian; Ye, Deju; Liu, Hong; Luo, Xiaoming; Jiang, Hualiang
Synthetic Communications, 2008 , vol. 38, # 4 p. 567 - 575
参考文献
Bahner et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 3499
反应条件
1.1: anhydrous potassium carbonate / CHCl3 / Heating
2.1: Br2; sodium acetate; acetic acid / 3 h
2.2: 48.3 percent / ethanol / 8 h / Heating
View Scheme
参考文献
Ling, Shao; Xin, Zhou; Qing, Zhang; Jian-Bing, Liu; Zhong, Jin; Jian-Xin, Fang
Synthetic Communications, 2007 , vol. 37, # 2 p. 199 - 207
反应条件
in ethanol; water
T=20°C;
参考文献
Lee, Sunkyung; Kim, Taemi; Lee, Byung Ho; Yoo, Sung-eun; Lee, Kyunghee; Yi, Kyu Yang
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 5 p. 1291 - 1295
