2,3-二氢苯并[b]噻吩合成路线 （共 7 条）
反应条件
vanadium pentaoxide; [C12mim][HSO4]; dihydrogen peroxide in water T=45°C; 8 h;
参考文献
Hu, Yu-Lin; Liu, Xiao-Bing; Fang, Dong
Catalysis Science and Technology, 2014 , vol. 4, # 1 p. 38 - 42
反应条件
titanium(IV) isopropylate; alpha,alpha-dimethylbenzyl hydroperoxide; C22H30O12 in dichloromethane; water T=-20°C; 12 h; Inert atmosphere; enantioselective reaction;
参考文献
Newhouse, Timothy R.; Li, Xin; Blewett, Megan M.; Whitehead, Clare M. C.; Corey
Journal of the American Chemical Society, 2012 , vol. 134, # 42 p. 17354 - 17357
反应条件
sodium periodate in ethanol Yield given. Yields of byproduct given;
参考文献
Allenmark, Stig G.; Andersson, Malin A.
Tetrahedron Asymmetry, 1996 , vol. 7, # 4 p. 1089 - 1094
参考文献
Bianchini, Claudio; Meli, Andrea; Oberhauser, Werner; Vizza, Francesco
Chemical Communications, 1999 , # 8 p. 671 - 672
反应条件
hydrogen; aluminum oxide; cobalt; molybdenum in decane T=269.9°C; P=750.06 Torr; study of hydrodesulphurization, other catalysts; KineticsEquilibrium constant;
参考文献
Peter, Rudolf; Matejec, Vlastimil; Zdrazil, Miroslav
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 6 p. 1195 - 1205
反应条件
Titanium(IV) oxide; silver sulphate in acetonitrile T=20°C; 2 h; UV-irradiation; Title compound not separated from byproducts;
参考文献
Journal of Physical Organic Chemistry, , vol. 19, # 6 p. 359 - 364
反应条件
1: 49 percent / AlCl3 / CH2Cl2 / 0.5 h / -6 °C 2: sulfur, p-toluenesulfonic acid / 5 h / Heating 3: 78 percent / HOAc, H2SO4, H2O / 4 h / Heating 4: conc. H2SO4 / toluene / 3 h / Heating 5: AlCl3 / CS2 / 2 h / Heating 6: aq. NaOH / methanol / 2 h / Heating View Scheme
参考文献
Dunn; Ackerman; Tomolonis
Journal of Medicinal Chemistry, 1986 , vol. 29, # 11 p. 2326 - 2329
