(双(三甲基甲硅烷基))碲化合成路线 (共 19 条)
反应条件
lithium telluride in diethyl ether
参考文献
Drake, John E.; Glavincevski, Boris M.; Hemmings, Raymond T.
Canadian Journal of Chemistry, 1980 , vol. 58, # 20 p. 2161 - 2166
反应条件
Te-powder 336 h; Ambient temperature;
参考文献
Mont, Wolf-Walther du; Severengiz, Tevfik; Meyer, Bernd
Angewandte Chemie, 1983 , vol. 95, # 12 p. 1025 - 1026
反应条件
in not given room temp.; followed by (1)H NMR;
参考文献
Bonasia, Philip J.; Gindelberger, David E.; Arnold, John
Inorganic Chemistry, 1993 , vol. 32, p. 5126 - 5131
反应条件
in neat (no solvent) 18 h at room temp.;
参考文献
Eujen, R.; Laufs, F. E.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1988 , vol. 561, p. 82 - 98
反应条件
tellurium 1.) THF, 2.) THF, RT, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Jones, C. H. W.; Sharma, R. D.
Journal of Organometallic Chemistry, 1984 , vol. 268, # 2 p. 113 - 118
参考文献
Mont, Wolf-Walther du; Severengiz, Tevfik; Meyer, Bernd
Angewandte Chemie, 1983 , vol. 95, # 12 p. 1025 - 1026
反应条件
tellurium 1.) THF, 2.) THF, RT, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Jones, C. H. W.; Sharma, R. D.
Journal of Organometallic Chemistry, 1984 , vol. 268, # 2 p. 113 - 118
参考文献
Mont, Wolf- Walther du
Angewandte Chemie, 1980 , vol. 92, # 7 p. 562 - 563
反应条件
condensation of (CF3)3GeF on (Si(CH3)3)2Te in a glass tube, warming to room temp. under exclusion of light for 12 h; fractionation in high vac.; elem. anal.;
参考文献
Eujen, R.; Laufs, F. E.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1988 , vol. 561, p. 82 - 98
反应条件
hydrogen sulfide
2 h; Title compound not separated from byproducts;
参考文献
Drake, John E.; Glavincevski, Boris M.; Hemmings, Raymond T.
Canadian Journal of Chemistry, 1980 , vol. 58, # 20 p. 2161 - 2166