1-甲氧基-3-甲基-9h-咔唑合成路线 （共 43 条）
反应条件
potassium phosphate; tri-cyclo-hexyl-phosphine; palladium diacetate in 1-methyl-pyrrolidin-2-one
T=130°C; 18 h;
参考文献
Ackermann, Lutz; Althammer, Andreas; Mayer, Peter
Synthesis, 2009 , # 20 p. 3493 - 3503
反应条件
potassium phosphate; tri-cyclo-hexyl-phosphine; palladium diacetate in 1-methyl-pyrrolidin-2-one
T=130°C; 18 h;
参考文献
Ackermann, Lutz; Althammer, Andreas; Mayer, Peter
Synthesis, 2009 , # 20 p. 3493 - 3503
反应条件
copper diacetate; palladium diacetate in N,N-dimethyl-formamide
T=130°C; 1 h; Sealed tubeMicrowave irradiation;
参考文献
Sridharan, Vellaisamy; Antonia Martin; Carlos Menendez
European Journal of Organic Chemistry, 2009 , # 27 p. 4614 - 4621
反应条件
lithium aluminium tetrahydride in diethyl ether; dichloromethane
T=20°C; 4.5 h;
参考文献
Thomas, Claudia; Knoelker, Hans-Joachim
Tetrahedron Letters, 2013 , vol. 54, # 6 p. 591 - 593
反应条件
copper(l) iodide in N,N-dimethyl-formamide
T=120°C; 3 h;
参考文献
Kikugawa; Aoki; Sakamoto
Journal of Organic Chemistry, 2001 , vol. 66, # 25 p. 8612 - 8615
反应条件
1: With magnesium sulphate heptahydrate in methanol; dichloromethane
2: With sodium tetrahydroborate; palladium 10 on activated carbon
T=100°C; P=1551.49 - 2585.81 Torr; 0.0666667 h; Microwave irradiation;
参考文献
Chakraborty, Suchandra; Chattopadhyay, Gautam; Saha, Chandan
Journal of Heterocyclic Chemistry, 2013 , vol. 50, # 1 p. 91 - 98
反应条件
trifluorormethanesulfonic acid; trifluoroacetic acid
0.25 h; Heating;
参考文献
Mal, Dipakranjan; Senapati, Bidyut Kumar; Pahari, Pallab
Tetrahedron, 2007 , vol. 63, # 18 p. 3768 - 3781
反应条件
lithium aluminium tetrahydride; aluminium trichloride in diethyl ether; dichloromethane
T=0 - 20°C;
参考文献
Bringmann, Gerhard; Tasler, Stefan
Tetrahedron, 2001 , vol. 57, # 12 p. 2337 - 2343
反应条件
1: 93 percent / K2CO3 / acetone / 3 h / Heating
2: 71 percent / glacial acetic acid / Pd(OAc)2 / 10 h / 140 °C
View Scheme
参考文献
Benavides, Adriana; Peralta, Javier; Delgado, Francisco; Tamariz, Joaquin
Synthesis, 2004 , # 15 p. 2499 - 2504
反应条件
in diethyl ether
T=5°C; 24 h;
参考文献
Bringmann, Gerhard; Ledermann, Alfons; Francois, Guido
Heterocycles, 1995 , vol. 40, # 1 p. 293 - 300
