2-甲基-3-丁烯-1-醇合成路线 （共 21 条）
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane); hydroxide; dihydrogen peroxide 1.) THF, r.t., 6 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Zaidlewicz, Marek; Meller, Jerzy
Tetrahedron Letters, 1997 , vol. 38, # 41 p. 7279 - 7282
反应条件
(i) CuI, (ii) /BRN= 103170/; Multistep reaction;
参考文献
Johnson,C.R. et al.
Journal of Organic Chemistry, 1973 , vol. 38, # 25 p. 4263 - 4268
反应条件
(i) pentane, (ii) H2NCH2CH2OH; Multistep reaction;
参考文献
Kramer,G.W.; Brown,H.C.
Journal of Organic Chemistry, 1977 , vol. 42, p. 2292 - 2299
反应条件
Sm{N(SiMe3)2}3 23 h; Ambient temperaturefurther organoyttrium- and organolanthanoid-reagents; Product distribution;
参考文献
Mukerji, Ishita; Wayda, Andrea L.; Dabbagh, Gary; Bertz, Steven H.
Angewandte Chemie, 1986 , vol. 98, # 8 p. 756 - 757
反应条件
dilithium tetrachlorocuprate; magnesium 1.) Et2O, 2.) Et2O/THF, -78 deg C, then room temp.; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Daradics, L.; Oprean, I.; Hodosan, F.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 2 p. 277 - 282
反应条件
in diethyl ether 23 h; Ambient temperature;
参考文献
Mukerji, Ishita; Wayda, Andrea L.; Dabbagh, Gary; Bertz, Steven H.
Angewandte Chemie, 1986 , vol. 98, # 8 p. 756 - 757
反应条件
(i) Al, HgCl2, ZnCl2, MeI, (ii) chloral; Multistep reaction;
参考文献
Sumitani,M. et al.
Bulletin of the Chemical Society of Japan, 1978 , vol. 51, p. 1511 - 1515
反应条件
(i) Mg, Et2O, (ii) /BRN= 1209228/, (iii) H2O; Multistep reaction;
参考文献
Piancatelli,G.; Scettri,A.
Gazzetta Chimica Italiana, 1974 , vol. 104, p. 343 - 356
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane T=25°C; 12 h;
参考文献
Negishi,E.; Boardman,L.D.; Sawada,H.
Journal of the American Chemical Society, 1988 , vol. 110, p. 5383
反应条件
in dichloromethane; N,N-dimethyl-formamide
参考文献
Merck and Co., Inc.
Patent: US5830875 A1, 1998 ;
