2-甲基-3-丁烯-1-醇合成路线 (共 21 条)
反应条件
ammonium chloride; magnesium; paraformaldehyde in (2S)-N-methyl-1-phenylpropan-2-amine hydrate
参考文献
Ortho Pharmaceutical Corp.
Patent: US4182717 A1, 1980 ;
反应条件
dimethylaluminum chloride in dichloromethane T=25°C; 0.416667 h; Title compound not separated from byproducts;
参考文献
Snider; Rodini; Kirk; Cordova
Journal of the American Chemical Society, 1982 , vol. 104, # 2 p. 555 - 563
反应条件
dimethylaluminum chloride in dichloromethane T=25°C; 0.416667 h; Title compound not separated from byproducts;
参考文献
Snider; Rodini; Kirk; Cordova
Journal of the American Chemical Society, 1982 , vol. 104, # 2 p. 555 - 563
反应条件
lithium aluminium tetrahydride
参考文献
Bloodworth; Curtis; Spencer; Tallant
Tetrahedron, 1993 , vol. 49, # 13 p. 2729 - 2750
反应条件
tin in tetrahydrofuran; water Ambient temperatureIrradiation;
参考文献
Einhorn, Cathy; Luche, Jean-Louis
Journal of Organometallic Chemistry, 1987 , vol. 322, p. 177 - 184
参考文献
Roberts; Young
Journal of the American Chemical Society, 1945 , vol. 67, p. 150
Full Text Show Details
Inhoffen; Bohlmann; Reinefeld
Chemische Berichte, 1949 , vol. 82, p. 315
反应条件
in tetrahydrofuran T=-40°C; 4 h; Yield given. Yields of byproduct given;
参考文献
Bourgain-Commercon, Monique; Normant, Jean F.
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 5-6 p. 289 - 294
反应条件
in diethyl ether Heating;
参考文献
Ashcroft, Martyn R.; Bury, Adrian; Cooksey, Christopher J.; Davies, Alwyn G.; Gupta, B. Dass; et al.
Journal of Organometallic Chemistry, 1980 , vol. 195, # 1 p. 89 - 104
反应条件
copper(I) bromide in tetrahydrofuran
参考文献
Normant,J.F. et al.
Tetrahedron Letters, 1978 , p. 3711 - 3712
反应条件
lithium aluminium tetrahydride
参考文献
Miginiac,P.; Zamlouty,G.
Journal of Organometallic Chemistry, 1975 , vol. 96, p. 163 - 168