N-Cbz-DL-天冬氨酸合成路线 (共 10 条)
反应条件
magnesium oxide in diethyl ether; water
参考文献
The Penn State Research Foundation
Patent: EP1420021 A1, 2004 ;
Location in patent: Page 15-16 ;
反应条件
water; magnesium oxide; benzyl chloroformate Reagens 4: Aether;
参考文献
Adembri; Ghelardoni
Gazzetta Chimica Italiana, 1959 , vol. 89, p. 1763,1768
反应条件
citrate buffer; dl-cysteine hydrochloride; papain T=50°C; 24 h;
参考文献
Synthetic Communications, , vol. 18, # 4 p. 441 - 444
反应条件
resolved on CSP cellulose tris(3,5-dimethylphenylcarbamate) by chiral HPLC;
参考文献
Okamoto, Yoshio; Aburatani, Ryo; Kaida, Yuriko; Hatada, Koichi
Chemistry Letters, 1988 , p. 1125 - 1128
反应条件
McIlvaine buffer; triethylamine; papain in ethyl acetate T=37°C; 72 h;
参考文献
Chen, S. T.; Wang, K. T.
Journal of Organic Chemistry, 1988 , vol. 53, # 19 p. 4589 - 4590
反应条件
McIlvaine buffer; triethylamine; papain in ethyl acetate T=37°C; 72 h;
参考文献
Chen, S. T.; Wang, K. T.
Journal of Organic Chemistry, 1988 , vol. 53, # 19 p. 4589 - 4590
反应条件
protease from Clostridium thermohydrosulfuricum SV 12 in phosphate buffer; ethyl acetate T=40°C; pH=6.5;
参考文献
Yadav; Meshram; Prasad; Ganesh; Rao; Seenayya; Swamy; Reddy
Tetrahedron Asymmetry, 2001 , vol. 12, # 18 p. 2505 - 2508
反应条件
dicyclohexyl-carbodiimide in ethyl acetate 1.) 1 h, 0 deg C, 2.) 24 h, r.t.;
参考文献
Munegumi, Toratane; Meng, Yan-Quing; Harada, Kaoru
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 8 p. 2748 - 2750
反应条件
resolved on CSP cellulose tris(3,5-dimethylphenylcarbamate) by chiral HPLC;
参考文献
Okamoto, Yoshio; Aburatani, Ryo; Kaida, Yuriko; Hatada, Koichi
Chemistry Letters, 1988 , p. 1125 - 1128
反应条件
sodium hypochlorite in methanol; water
Heating;
参考文献
Seki, Masahiko; Moriya, Tamon; Matsumoto, Kazuo
Agricultural and Biological Chemistry, 1984 , vol. 48, # 5 p. 1251 - 1256