N-(氯苯基亚甲基)-苯磺酰胺合成路线 （共 10 条）
反应条件
1: 73 percent / benzene / 2 h / 70 - 80 °C 2: 82 percent / trityl perchlorate / acetonitrile / 0.25 h / Heating 3: 50 percent / acetonitrile / 1 h / Heating View Scheme
参考文献
Sheinkman, A. K.; Kozak, I. Yu.; Zemskii, B. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 7 p. 768 - 772
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 7 p. 955 - 960
参考文献
Mikhailov, B. A.; Drizhd, L. P.; Litvinenko, L. M.; Bondarenko, L. I.; Savelova, V. A.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 7 p. 1309 - 1313
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 7 p. 1456 - 1461
反应条件
ammonia in diethyl ether T=-15°C; 0.333333 h;
参考文献
Yagupolskii, Lev M.; Maletina, Irina I.; Sokolenko, Liubov V.; Vlasenko, Yurii G.; Buth, Sergey A.
Journal of Fluorine Chemistry, 2008 , vol. 129, # 6 p. 486 - 492
反应条件
(i) NaOAc, (ii) (heating in benzene); Multistep reaction;
参考文献
Dubina,V.L. et al.
Zhurnal Organicheskoi Khimii, 1971 , vol. 7, p. 358 - 362,354 - 357
反应条件
bei der Destillation;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 214, p. 212
反应条件
1: 59 percent / benzene / 2 h / 70 - 80 °C 2: 60 percent / (C6H5)3C(1+)*ClO4(1-) / acetonitrile / 0.08 h / Heating 3: 60 percent / 20percent aq.KOH / ethanol / 2.5 h / Heating View Scheme
参考文献
Sheinkman, A. K.; Kozak, I. Yu.; Zemskii, B. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 7 p. 768 - 772
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 7 p. 955 - 960
反应条件
sodium azide in ethylene glycol dimethyl ether
T=48 - 50°C; 2 h;
参考文献
Yagupolskii, Lev M.; Shelyazhenko, Svetlana V.; Maletina, Irina I.; Petrik, Vitalij N.; Rusanov, Eduard B.; Chernega, Alexander N.
European Journal of Organic Chemistry, 2001 , # 7 p. 1225 - 1233
参考文献
Wallach
Justus Liebigs Annalen der Chemie, 1882 , vol. 214, p. 212
反应条件
bei der Destillation;
参考文献
Wallach
Justus Liebigs Annalen der Chemie, 1882 , vol. 214, p. 212
反应条件
diazomethane; morpholine; lithium chloride
Inert atmosphere;
参考文献
Yagupolskii, Lev M.; Maletina, Irina I.; Sokolenko, Liubov V.; Vlasenko, Yurii G.; Drozdova, Maria V.; Polovinko, Vitaliy V.
Journal of Fluorine Chemistry, 2010 , vol. 131, # 2 p. 238 - 247
