2,2,4-三甲基-1,2,3,4-四氢喹啉合成路线 （共 8 条）
反应条件
hydrogen; palladium on activated charcoal in ethanol T=20°C; 5 h;
参考文献
Oka, Hiroyuki; Tamura, Tomoki; Miura, Yozo; Teki, Yoshio
Journal of Materials Chemistry, 2001 , vol. 11, # 5 p. 1364 - 1369
反应条件
hydrogen; nickel in ethanol T=100°C; P=2280 Torr; 62 h;
参考文献
Terada; Takeuchi; Hamada
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 5 p. 1917 - 1923
反应条件
1: 60 percent / NaH / dimethylsulfoxide / 3.5 h / 70 °C 2: 72 percent / HCl / Zn-Hg / acetic acid / 1 h / 95 °C 3: 58 percent / H2 / Raney Ni / ethanol / 62 h / 100 °C / 2280 Torr View Scheme
参考文献
Terada; Takeuchi; Hamada
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 5 p. 1917 - 1923
反应条件
1: 72 percent / HCl / Zn-Hg / acetic acid / 1 h / 95 °C 2: 58 percent / H2 / Raney Ni / ethanol / 62 h / 100 °C / 2280 Torr View Scheme
参考文献
Terada; Takeuchi; Hamada
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 5 p. 1917 - 1923
反应条件
1: iodine / 170 - 180 °C / im Rohr 2: nickel; silicon dioxide / 100 °C / 7600 Torr / Hydrogenation View Scheme
参考文献
Cheng, Ming; Yang, Xichuan; Li, Jiajia; Chen, Cheng; Zhao, Jianghua; Wang, Yu; Sun, Licheng
Chemistry - A European Journal, 2012 , vol. 18, # 50 p. 16196 - 16202
参考文献
Schlenk; Bergmann
Justus Liebigs Annalen der Chemie, 1928 , vol. 463, p. 208
Full Text Show Details
Reddelien; Thurm
Chemische Berichte, 1932 , vol. 65, p. 1514
Full Text Show Details
Knoevenagel
Chemische Berichte, 1922 , vol. 55, p. 2318
反应条件
TEA in chloroform T=20°C; 18 h;
参考文献
Zhao, He; Thurkauf, Andrew; He, Xiaoshu; Hodgetts, Kevin; Zhang, Xiaoyan; Rachwal, Stanislaw; Kover, Renata X.; Hutchison, Alan; Peterson, John; Kieltyka, Andrzej; Brodbeck, Robbin; Primus, Renee; Wasley, Jan W.F.
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 21 p. 3105 - 3109
反应条件
in benzene
2 h; Reflux;
参考文献
Cheng, Ming; Yang, Xichuan; Li, Jiajia; Zhang, Fuguo; Sun, Licheng
ChemSusChem, 2013 , vol. 6, # 1 p. 70 - 77
