3-甲基-1-苯基-2-丁烯合成路线 (共 98 条)
反应条件
bei der Ozonspaltung;
参考文献
Staudinger; Kreis; Schilt
Helvetica Chimica Acta, 1922 , vol. 5, p. 750
反应条件
Grubb's 2nd generation catalyst; toluene-4-sulfonic acid in water T=22°C; 12 h; Sealed vialInert atmosphere;
参考文献
Lipshutz, Bruce H.; Ghorai, Subir; Leong, Wendy Wen Yi; Taft, Benjamin R.; Krogstad, Daniel V.
Journal of Organic Chemistry, 2011 , vol. 76, # 12 p. 5061 - 5073
参考文献
Claisen
Journal fuer Praktische Chemie (Leipzig), 1922 , vol. <2> 105, p. 72
Chemische Berichte, 1925 , vol. 58, p. 279 Anm. 15
反应条件
silver hexafluoroantimonate; 1,10-phenanthroline; palladium diacetate in 1,2-dichloro-ethane
T=60°C; 12 h; Inert atmosphere; regiospecific reaction;
参考文献
Ohmiya, Hirohisa; Makida, Yusuke; Tanaka, Tatsunori; Sawamura, Masaya
Journal of the American Chemical Society, 2008 , vol. 130, # 51 p. 17276 - 17277
反应条件
lithium chloride; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide
T=23°C; 27 h;
参考文献
Valle, L. Del; Stille, J. K.; Hegedus, L. S.
Journal of Organic Chemistry, 1990 , vol. 55, p. 3019 - 3023
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
1 h; Ambient temperature;
参考文献
Matsushita,H.; Negishi,E.I.
Journal of the American Chemical Society, 1981 , vol. 103, p. 2882
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in toluene
T=110°C; Suzuki-Miyaura coupling; 17 h; Inert atmosphere;
参考文献
Gerbino, Dario C.; Mandolesi, Sandra D.; Schmalz, Hans-Guenther; Podesta, Julio C.
European Journal of Organic Chemistry, 2009 , # 23 p. 3964 - 3972
反应条件
formic acid; triethylamine; palladium on activated charcoal
T=25°C; 72 h;
参考文献
Weir, John R.; Patel, Babu A.; Heck, Richard F.
Journal of Organic Chemistry, 1980 , vol. 45, # 24 p. 4926 - 4931
反应条件
metalloprotein-inspired polymeric imidazole/palladium in water; isopropyl alcohol
T=50°C; 4 h;
参考文献
Yamada, Yoichi M. A.; Sarkar, Shaheen M.; Uozumi, Yasuhiro
Journal of the American Chemical Society, 2012 , vol. 134, # 6 p. 3190 - 3198
反应条件
toluene-4-sulfonic acid in toluene
5 h; Heating; Yield given. Yields of byproduct given;
参考文献
Von Doering; Benkhoff, Johannes; Carleton, Peter Smart; Pagnotta, Marco
Journal of the American Chemical Society, 1997 , vol. 119, # 45 p. 10947 - 10955