trifluorormethanesulfonic acid in tetrachloromethane P=87400.1 Torr; 3 h; Ambient temperature; Further byproducts given;
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Booth, Brian L.; El-Fekky, Teymour A.; Noori, Ghazi F. M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 181 - 186
1: 93 percent / LiAlH4 / diethyl ether 2: D3PO4 / 3 h / 230 - 240 °C View Scheme
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Sakhabutdinov, A. G.; Usmanova, A. G.; Frolov, P. A.; Kushnarev, D. F.; Schmidt, F. K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 8 p. 1452 - 1455
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1610 - 1614
1.1: n-butyllithium / tetrahydrofuran; hexane / 0 °C / Inert atmosphere 1.2: 3.83 h / -78 - 20 °C / Inert atmosphere 2.1: 5 Pd(II)/C(eggshell); hydrogen / ethanol / 18 h / 45 °C / 3040.2 Torr View Scheme
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Monfette, Sebastien; Turner, Zoe R.; Semproni, Scott P.; Chirik, Paul J.
Journal of the American Chemical Society, 2012 , vol. 134, # 10 p. 4561 - 4564
phosphoric acid, fully deuterated T=230 - 240°C; 3 h; Yield given. Title compound not separated from byproducts;
参考文献
Sakhabutdinov, A. G.; Usmanova, A. G.; Frolov, P. A.; Kushnarev, D. F.; Schmidt, F. K.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 8 p. 1452 - 1455
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 8 p. 1610 - 1614
Konowalow; Jegorow
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1898 , vol. 30, p. 1031
Chem. Zentralbl., 1899 , vol. 70, # I p. 776
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Gleditsch
Bulletin de la Societe Chimique de France, 1906 , vol. <3> 35, p. 1095
