N,N-二甲基甲酰胺-d7合成路线 （共 7 条）
反应条件
in diethyl ether 1.5 h;
参考文献
Gruttadauria, Michelangelo; Meo, Paolo Lo; Noto, Renato; Werber, Giuseppe
Gazzetta Chimica Italiana, 1997 , vol. 127, # 5 p. 277 - 282
反应条件
T=70°C; 3 h; Product distributionRate constant;
参考文献
Chemische Berichte, , vol. 120, p. 217 - 224
反应条件
in neat (no solvent) Irradiation (UV/VIS); a soln. of complex photolysed, reacted with (13)CO2, monitored by NMR, FTIR and GC; not isolated;
参考文献
Hayashi, Yukiko; Kita, Shouichi; Brunschwig, Bruce S.; Fujita, Etsuko
Journal of the American Chemical Society, 2003 , vol. 125, # 39 p. 11976 - 11987
反应条件
cerium(IV) oxide T=180°C; 8 h; Sealed tube; Temperature;
参考文献
Wang, Yehong; Wang, Feng; Zhang, Chaofeng; Zhang, Jian; Li, Mingrun; Xu, Jie
Chemical Communications, 2014 , vol. 50, # 19 p. 2438 - 2441
反应条件
in DMF-d7
byproducts: (CH3)3COH, KCl; (Ar); addn. of fluoroform to mixt. of copper chloride and potassium tert-butoxide in DMF-d7 at room temp.; NMR monitoring;
参考文献
Zanardi, Alessandro; Novikov, Maxim A.; Martin, Eddy; Benet-Buchholz, Jordi; Grushin, Vladimir V.
Journal of the American Chemical Society, 2011 , vol. 133, # 51 p. 20901 - 20913
反应条件
bis(cyclopentadienyl)titanium dichloride; sodium tetrahydroborate
1.) 96 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Liu, Yumin; Schwartz, Jeffrey
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 5005 - 5007
反应条件
di-tert-butyl peroxide; copper diacetate
T=110°C; 3 h; Schlenk techniqueInert atmosphere;
参考文献
Wang, Hua; Guo, Li-Na; Duan, Xin-Hua
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 28 p. 4573 - 4576
