3-甲基-1,5-戊二醇合成路线 （共 33 条）
反应条件
T=250°C; unter Druck;
参考文献
Paden; Adkins
Journal of the American Chemical Society, 1936 , vol. 58, p. 249
反应条件
carbon tetrabromide; triphenylphosphine in dichloromethane T=0°C; 1 h;
参考文献
Mladkova, Jana; Vanek, Vaclav; Budesinsky, Milos; Elbert, Tomas; Demianova, Zuzana; Garrow, Timothy A.; Jiracek, Jiri
Journal of Medicinal Chemistry, 2012 , vol. 55, # 15 p. 6822 - 6831
反应条件
Dowex 50W x 2 in toluene T=30°C; Etherification; hydration; 1.66667 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 23 p. 8183 - 8187
反应条件
dinitrogen tetraoxide in nitric acid T=60°C; Heating;
参考文献
Journal of Organic Chemistry, , vol. 45, # 2 p. 247 - 250
反应条件
T=250°C; unter Druck;
参考文献
Paden; Adkins
Journal of the American Chemical Society, 1936 , vol. 58, p. 249
反应条件
dinitrogen tetraoxide in nitric acid T=60°C; Heating;
参考文献
Wilkes, John B.; Wall, Robert G.
Journal of Organic Chemistry, 1980 , vol. 45, # 2 p. 247 - 250
反应条件
sodium hydroxide; benzenesulfonic Acid
参考文献
BASF Aktiengesellschaft
Patent: US5001242 A1, 1991 ;
反应条件
1: PBr3
2: NaNH2 / diethyl ether; liquid ammonia
View Scheme
参考文献
Cope,A.C.; Gale,D.M.
Journal of the American Chemical Society, 1963 , vol. 85, p. 3743 - 3747
参考文献
Eliel, Ernest L.; Manoharan, Muthiah; Pietrusiewicz, K. Michal; Hargrave, Karl D.
Organic Magnetic Resonance, 1983 , vol. 21, # 2 p. 94 - 107
反应条件
phosphorus; iodine
T=45°C; 42 h; Cooling with ice bath;
参考文献
Jahangir, Alam; Lynch, Stephen M.; Soth, Michael; Yang, Hanbiao
Patent: US2011/71179 A1, 2011 ;
Location in patent: Page/Page column 31 ;
