1,3-苯并二氧杂环戊烯-5-乙腈合成路线 (共 43 条)
反应条件
copper(l) iodide in toluene T=180°C; 20 h; Inert atmosphereSealed tube;
参考文献
Tetrahedron Letters, , vol. 53, # 23 p. 2825 - 2827
反应条件
sodium hydrogen telluride; acetic acid in ethanol; benzene T=-20°C; 0.333333 h;
参考文献
Tetrahedron, , vol. 52, # 25 p. 8611 - 8618
反应条件
2,2,6,6-tetramethyl-piperidine-N-oxyl; free radical; trichloroisocyanuric acid in dichloromethane T=10°C; 2.5 h;
参考文献
Synthesis, , # 17 p. 2629 - 2631
反应条件
dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; bis(η3-allyl-μ-chloropalladium(II)) in 1,3,5-trimethyl-benzene T=20 - 140°C; 5.16667 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 19 p. 4470 - 4474
反应条件
1: SOCl2 / dioxane / 20 °C 2: acetonitrile / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 11, # 16 p. 2205 - 2208
反应条件
acetic acid; zinc T=100°C; 1 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 10 p. 3574 - 3579
反应条件
tetrachloromethane; 18-crown-6 ether; tributylphosphine in acetonitrile 24 h; Ambient temperature;
参考文献
Synthesis, , # 12 p. 1007 - 1009
反应条件
titanium tetrachloride; tetraethylammonium p-toluenesulfonate in N,N-dimethyl-formamide electroreduction - 4 mA/cm2;
参考文献
Synthesis, , # 7 p. 631 - 633
反应条件
tetrabutylammomium bromide in chloroform; water T=20 - 60°C; 2 h;
参考文献
Chemistry - An Asian Journal, , vol. 8, # 9 p. 1966 - 1971
反应条件
acetone; sodium iodide
参考文献
DE896344 , ;
DRP/DRBP Org.Chem.