2-甲基-3-苯基环氧乙烷合成路线 （共 22 条）
反应条件
lithium diisopropyl amide in tetrahydrofuran; diethyl ether 24 h; Ambient temperature;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 4 p. 1179 - 1184
反应条件
aluminum oxide; sodium tetrahydroborate; palladium dichloride in hexane; water T=30°C; 1 h;
参考文献
Yakabe, Shigetaka
Synthetic Communications, 2010 , vol. 40, # 9 p. 1339 - 1344
反应条件
sodium tetrahydroborate in isopropyl alcohol 7 h; Heating; Yields of byproduct given;
参考文献
Ookawa, Atsuhiro; Hiratsuka, Hiroshi; Soai, Kenso
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, p. 1813 - 1818
反应条件
di-tert-butyl peroxide in neat (no solvent) addn. of peroxide to equimolar mixt. of (CH2CHCH2)4Sn and PhCHOCH2, 24h, 130°C, acidolysis by addn. of malonic acid in ether, reflux, 48h, ether removed, pptn. of malonate by addn. of pentane, under Ar; alcohol detected by chromy., total yield: 34percent;
参考文献
Daude, Gerard; Pereyre, Michel
Journal of Organometallic Chemistry, 1980 , vol. 190, # 1 p. 43 - 52
反应条件
carbon monoxide in tetrahydrofuran; water T=110°C; P=6840.46 Torr; 3 h; Autoclave; chemoselective reaction;
参考文献
Tetrahedron Letters, , vol. 51, # 41 p. 5466 - 5468
反应条件
Amberlite IRA-400; borohydride form; copper(II) sulfate in methanol T=20°C; Reduction; 3 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 70, # 5 p. 1101 - 1107
反应条件
sodium tetrahydroborate in isopropyl alcohol 7 h; Heating; Yields of byproduct given;
参考文献
Ookawa, Atsuhiro; Hiratsuka, Hiroshi; Soai, Kenso
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, p. 1813 - 1818
反应条件
indium(III) chloride in tetrahydrofuran T=25°C; Rearrangement; 0.833333 h;
参考文献
Journal of Organic Chemistry, , vol. 63, # 23 p. 8212 - 8216
反应条件
KH2F3 in 1,2-dichloro-ethane T=80°C; 12 h;
参考文献
Journal of Fluorine Chemistry, , vol. 70, # 1 p. 1 - 4
反应条件
boron trifluoride diethyl etherate in dichloromethane T=-50°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 70, # 16 p. 6541 - 6543
