2-苯基喹啉-4-羧酸乙酯合成路线 (共 11 条)
反应条件
di-isopropylperoxydicarbonate in benzene
T=60°C;
参考文献
Leardini, Rino; Pedulli, Gian Franco; Tundo, Antonio; Zanardi, Giuseppe
Journal of the Chemical Society, Chemical Communications, 1984 , # 20 p. 1320 - 1321
反应条件
sulfuric acid
0.166667 h; microwave irradiation;
参考文献
El Ashry, El Sayed H.; Ramadan, El Sayed; Hamid, Hamida Abdel; Hagar, Mohamed
Synthetic Communications, 2005 , vol. 35, # 17 p. 2243 - 2250
反应条件
ethanol; sulfuric acid
参考文献
Feist; et al.
Archiv der Pharmazie (Weinheim, Germany), 1938 , vol. 276, p. 271,278
Full Text Show Details
Gansser; Rumpf
Helvetica Chimica Acta, 1953 , vol. 36, p. 1423,1431
反应条件
indium(III) chloride in acetonitrile
aza-Diels-Alder reaction; 0.05 h; Heatingmicrowave irradiation;
参考文献
Duvelleroy, Dorothee; Perrio, Cecile; Parisel, Olivier; Lasne, Marie-Claire
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3794 - 3804
反应条件
1: 20 percent / InCl3 / acetonitrile / 0.05 h / Heating; microwave irradiation
View Scheme
参考文献
Duvelleroy, Dorothee; Perrio, Cecile; Parisel, Olivier; Lasne, Marie-Claire
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3794 - 3804
反应条件
1: 20 percent / InCl3 / acetonitrile / 0.05 h / Heating; microwave irradiation
View Scheme
参考文献
Duvelleroy, Dorothee; Perrio, Cecile; Parisel, Olivier; Lasne, Marie-Claire
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3794 - 3804
反应条件
indium(III) chloride in acetonitrile
aza-Diels-Alder reaction; 0.05 h; Heatingmicrowave irradiation;
参考文献
Duvelleroy, Dorothee; Perrio, Cecile; Parisel, Olivier; Lasne, Marie-Claire
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3794 - 3804
反应条件
indium(III) chloride in acetonitrile
aza-Diels-Alder reaction; 0.05 h; Heatingmicrowave irradiation; Title compound not separated from byproducts;
参考文献
Duvelleroy, Dorothee; Perrio, Cecile; Parisel, Olivier; Lasne, Marie-Claire
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3794 - 3804
反应条件
indium(III) chloride in acetonitrile
aza-Diels-Alder reaction; 0.05 h; Heatingmicrowave irradiation; Title compound not separated from byproducts;
参考文献
Duvelleroy, Dorothee; Perrio, Cecile; Parisel, Olivier; Lasne, Marie-Claire
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 20 p. 3794 - 3804
反应条件
1: 95 percent / potassium hydroxide / ethanol; H2O / 0.21 h / microwave irradiation
2: 94 percent / sulfuric acid / 0.17 h / microwave irradiation
View Scheme
参考文献
El Ashry, El Sayed H.; Ramadan, El Sayed; Hamid, Hamida Abdel; Hagar, Mohamed
Synthetic Communications, 2005 , vol. 35, # 17 p. 2243 - 2250