6,6′-二甲基-2,2′-联吡啶合成路线 （共 53 条）
反应条件
niobium bromide in N,N-dimethyl-formamide T=20°C; Electrochemical reactionconstant current intensity 200 mA;
参考文献
De Franca, Kelnner W. R.; Navarro, Marcelo; Leonel, Eric; Durandetti, Muriel; Nedelec, Jean-Yves
Journal of Organic Chemistry, 2002 , vol. 67, # 6 p. 1838 - 1842
反应条件
sodium hydroxide; palladium in methanol; water
参考文献
Axiva GmbH
Patent: US6500956 B1, 2002 ;
反应条件
(2,2′-bipyridine)nickel(II) dibromide; sodium iodide in N,N-dimethyl-formamide T=20°C; 8 h; Electrochemical reactionInert atmosphere;
参考文献
Oliveira, Jadson L.; Silva, Maria J.; Florencio, Tupolevck; Urgin, Karne; Sengmany, Stephane; Leonel, Eric; Nedelec, Jean-Yves; Navarro, Marcelo
Tetrahedron, 2012 , vol. 68, # 10 p. 2383 - 2390
反应条件
(2,2′-bipyridine)nickel(II) dibromide; sodium iodide in N,N-dimethyl-formamide T=20°C; 8 h; Electrochemical reactionInert atmosphere;
参考文献
Oliveira, Jadson L.; Silva, Maria J.; Florencio, Tupolevck; Urgin, Karne; Sengmany, Stephane; Leonel, Eric; Nedelec, Jean-Yves; Navarro, Marcelo
Tetrahedron, 2012 , vol. 68, # 10 p. 2383 - 2390
反应条件
nickel(II) dibromide hydrate; sodium iodide in N,N-dimethyl-formamide T=20°C; 8 h; Electrochemical reactionInert atmosphere;
参考文献
Oliveira, Jadson L.; Silva, Maria J.; Florencio, Tupolevck; Urgin, Karne; Sengmany, Stephane; Leonel, Eric; Nedelec, Jean-Yves; Navarro, Marcelo
Tetrahedron, 2012 , vol. 68, # 10 p. 2383 - 2390
反应条件
1.1: HBr; bromine / 2 h / -20 °C 1.2: 77 percent / sodium nitrite / H2O / 1.75 h / -20 - 15 °C 2.1: 50 percent / sodium formate; benzyltriethylammonium chloride; NaOH / Pd/C / H2O / 216 h / Heating View Scheme
参考文献
Laitinen, Riitta H.; Csoban, Katalin; Pursiainen, Jouni; Huuskonen, Juhani; Rissanen, Kari
Acta Chemica Scandinavica, 1997 , vol. 51, # 4 p. 462 - 469
反应条件
nickel(II) dibromide hydrate; sodium iodide in N,N-dimethyl-formamide T=20°C; Electrochemical reactionInert atmosphere;
参考文献
Oliveira, Jadson L.; Silva, Maria J.; Florencio, Tupolevck; Urgin, Karne; Sengmany, Stephane; Leonel, Eric; Nedelec, Jean-Yves; Navarro, Marcelo
Tetrahedron, 2012 , vol. 68, # 10 p. 2383 - 2390
反应条件
nickel(II) dibromide hydrate; sodium iodide in N,N-dimethyl-formamide T=20°C; Electrochemical reactionInert atmosphere;
参考文献
Oliveira, Jadson L.; Silva, Maria J.; Florencio, Tupolevck; Urgin, Karne; Sengmany, Stephane; Leonel, Eric; Nedelec, Jean-Yves; Navarro, Marcelo
Tetrahedron, 2012 , vol. 68, # 10 p. 2383 - 2390
反应条件
nickel(II) dibromide hydrate; sodium iodide in N,N-dimethyl-formamide T=20°C; Electrochemical reactionInert atmosphere;
参考文献
Oliveira, Jadson L.; Silva, Maria J.; Florencio, Tupolevck; Urgin, Karne; Sengmany, Stephane; Leonel, Eric; Nedelec, Jean-Yves; Navarro, Marcelo
Tetrahedron, 2012 , vol. 68, # 10 p. 2383 - 2390
反应条件
(2,2′-bipyridine)nickel(II) dibromide; sodium iodide in N,N-dimethyl-formamide T=20°C; 8 h; Electrochemical reactionInert atmosphere;
参考文献
Oliveira, Jadson L.; Silva, Maria J.; Florencio, Tupolevck; Urgin, Karne; Sengmany, Stephane; Leonel, Eric; Nedelec, Jean-Yves; Navarro, Marcelo
Tetrahedron, 2012 , vol. 68, # 10 p. 2383 - 2390
