苯基硼酸1,3-丙二醇酯合成路线 （共 23 条）
反应条件
copper(l) iodide; cesium fluoride in N,N-dimethyl-formamide T=120°C; Suzuki-Miyaura Coupling; 24 h; GloveboxInert atmosphere;
参考文献
Gurung, Santosh K.; Thapa, Surendra; Kafle, Arjun; Dickie, Diane A.; Giri, Ramesh
Organic Letters, 2014 , vol. 16, # 4 p. 1264 - 1267
反应条件
Au(Ph3P)+NTf2-; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile T=80°C; 0.25 h;
参考文献
Zhang, Guozhu; Peng, Yu; Cui, Li; Zhang, Liming
Angewandte Chemie, International Edition, 2009 , vol. 48, # 17 p. 3112 - 3115
反应条件
potassium tert-butylate; oxygen; (-)-sparteine; imidazole-carbene-derived Pd complex in isopropyl alcohol T=50°C; 24 h;
参考文献
Iwai, Yasumasa; Gligorich, Keith M.; Sigman, Matthew S.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 17 p. 3219 - 3222
反应条件
caesium carbonate; bis(dibenzylideneacetone)-palladium(0); tri-cyclo-hexyl-phosphine in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8) T=100°C; P=2660.18 Torr; 5 h;
参考文献
Ohashi, Masato; Saijo, Hiroki; Shibata, Mitsutoshi; Ogoshi, Sensuke
European Journal of Organic Chemistry, 2013 , # 3 p. 443 - 447
反应条件
copper diacetate; oxygen; triethylamine; 4 A molecular sieve in dichloromethane T=45°C; 20 h;
参考文献
Chernick, Erin T.; Ahrens, Michael J.; Scheidt, Karl A.; Wasielewski, Michael R.
Journal of Organic Chemistry, 2005 , vol. 70, # 4 p. 1486 - 1489
反应条件
1.1: tri-ruthenium(0)dodecacarbonyl / 3,3-dimethyl-butan-2-one / 24 h / 140 °C / Inert atmosphere 2.1: tetrahydrofuran / 20 °C 2.2: 20 °C 3.1: methyl trifluoromethanesulfonate / dichloromethane / 0 °C 3.2: 6 h / 50 °C View Scheme
参考文献
Dastbaravardeh, Navid; Schnuerch, Michael; Mihovilovic, Marko D.
Organic Letters, 2012 , vol. 14, # 7 p. 1930 - 1933
反应条件
copper diacetate; oxygen; triethylamine; 4 A molecular sieve in dichloromethane T=45°C; 20 h;
参考文献
Chernick, Erin T.; Ahrens, Michael J.; Scheidt, Karl A.; Wasielewski, Michael R.
Journal of Organic Chemistry, 2005 , vol. 70, # 4 p. 1486 - 1489
反应条件
water; bis(1,5-cyclooctadiene)nickel (0) in anhydrous butyl ether T=80°C; 24 h;
参考文献
Shirakawa; Takahashi; Tsuchimoto; Kawakami
Chemical Communications, 2001 , # 24 p. 2688 - 2689
反应条件
water; diphenyl acetylene; bis(1,5-cyclooctadiene)nickel (0) in 1,4-dioxane T=80°C; 24 h;
参考文献
Shirakawa, Eiji; Yasuhara, Yuichi; Hayashi, Tamio
Chemistry Letters, 2006 , vol. 35, # 7 p. 768 - 769
反应条件
potassium carbonate; Co0.38Fe0.57LaO3Pd0.05 in water; isopropyl alcohol T=80°C; Suzuki Coupling; 3 h; Product distribution / selectivity;
参考文献
US2005/215804 A1, ;
Page/Page column 16-17 ;
