1-苯基-2-丙烯-1-醇合成路线 (共 252 条)
反应条件
in tetrahydrofuran T=-10°C; 2 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 79, # 5 p. 2170 - 2177
反应条件
copper(l) iodide; zinc in ethanol sonication;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 12 p. 818 - 820
反应条件
tert.-butyl lithium in tetrahydrofuran T=-78 - 0°C; 1,2-Wittig rearrangement; 3 h;
参考文献
Organic Letters, , vol. 4, # 9 p. 1587 - 1590
反应条件
1: in tetrahydrofuran T=0 - 20°C; Inert atmosphere; 2: With water; ammonium chloride in tetrahydrofuran T=20°C;
参考文献
Tetrahedron, , vol. 64, # 51 p. 11745 - 11750
反应条件
magnesium in methanol T=-23°C;
参考文献
Journal of Organic Chemistry, , vol. 58, # 6 p. 1523 - 1530
反应条件
1.1: 70 percent / PBu3 / tetrahydrofuran 2.1: 4 Angstroem molecular sieves; cumene hydroperoxide / vanadyl acetylacetonate / CH2Cl2 / 0.5 h / -10 °C 2.2: 65 percent / Bu3P / CH2Cl2 / 0.08 h / -10 °C View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 2, # 9 p. 1315 - 1329
反应条件
tris(acetonitrile)(η5-2,4-cyclopentadien-1-yl)ruthenium(1+) hexafluorophosphate(1-); potassium carbonate; 3,4,5-trimethoxyphenylboronic acid in acetonitrile T=20°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Chemistry - A European Journal, , vol. 14, # 18 p. 5630 - 5637
反应条件
sodium carbonate; ethylene glycol; 3-chloro-benzenecarboperoxoic acid in chloroform T=-17 - -13°C;
参考文献
Journal of the American Chemical Society, , vol. 105, # 9 p. 2908 - 2909
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; poly(dibutylstannane); dibutyltin difluoride in tetrahydrofuran T=20°C; Reduction;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 72, # 3 p. 465 - 470
反应条件
potassium tert-butylate in tetrahydrofuran T=-78 - 0°C; Ramberg-Baecklund reaction;
参考文献
Tetrahedron Letters, , vol. 44, # 7 p. 1473 - 1475