1-苯基-2-丙烯-1-醇合成路线 (共 252 条)
反应条件
1: in tetrahydrofuran T=0 - 20°C; Inert atmosphere; 2: With ammonium chloride in water
参考文献
Angewandte Chemie - International Edition, , vol. 47, # 48 p. 9284 - 9288
反应条件
1: With 1,1'-bis-(diphenylphosphino)ferrocene; CuF(PPh3)3 in N,N-dimethyl-formamide T=60°C; 3 h; 2: With tetrabutyl ammonium fluoride in tetrahydrofuran; N,N-dimethyl-formamide T=20°C; 0.166667 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 12 p. 4138 - 4139
反应条件
1: benzoic acid ethyl ester With LDBBA in tetrahydrofuran; hexane T=0°C; 2: vinyl-magnesium bromide in tetrahydrofuran; diethyl ether; hexane T=20°C; 3: With hydrogenchloride; water in tetrahydrofuran; diethyl ether; hexane
参考文献
Tetrahedron Letters, , vol. 52, # 14 p. 1718 - 1720
反应条件
pyridine; hydrogen T=25°C; P=760.051 Torr; 6 h; Green chemistry; chemoselective reaction;
参考文献
ChemCatChem, , vol. 5, # 8 p. 2360 - 2366
反应条件
1: With alpha,alpha-dimethylbenzyl hydroperoxide; 4 A molecular sieve; vanadyl acetylacetonate in dichloromethane T=-10°C; 0.5 h; 2: With tributylphosphine in dichloromethane T=-10°C; 0.0833333 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 2, # 9 p. 1315 - 1329
反应条件
1: With alpha,alpha-dimethylbenzyl hydroperoxide; 4 A molecular sieve; vanadyl acetylacetonate in dichloromethane T=-10°C; 0.5 h; 2: With tributylphosphine in dichloromethane T=-10°C; 0.0833333 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 2, # 9 p. 1315 - 1329
反应条件
in tetrahydrofuran T=0 - 20°C; Grignard reaction; 0.666667 h;
参考文献
Tetrahedron Letters, , vol. 50, # 48 p. 6676 - 6679
反应条件
chromium dichloride in N,N-dimethyl-formamide T=25°C; 15 h;
参考文献
Tetrahedron Letters, , vol. 24, # 47 p. 5281 - 5284
反应条件
phthalic acid bis-(2-ethyl-hexyl)-ester T=30°C; pH=6.5; 24 h; aq. phosphate buffer; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 22, # 2 p. 134 - 137
反应条件
potassium carbonate; 3,4,5-trimethoxyphenylboronic acid; [Ru(cyclopentadienyl)(MeCN)3]PF6 in acetonitrile T=20°C; 16 h;
参考文献
New Journal of Chemistry, , vol. 32, # 6 p. 929 - 931