6-氰基-2,2'-联吡啶合成路线 （共 14 条）
反应条件
benzoyl chloride in dichloromethane T=0 - 20°C;
参考文献
Tse, Man Kin; Jiao, Haijun; Anilkumar, Gopinathan; Bitterlich, Bianca; Gelalcha, Feyissa Gadissa; Beller, Matthias
Journal of Organometallic Chemistry, 2006 , vol. 691, # 21 p. 4419 - 4433
反应条件
η5-cyclopentadienyl-η4-cycloocta-1,5-diene-cobalt(I) in toluene T=100°C; P=9880 Torr; 48 h;
参考文献
Chelucci, Giorgio; Cabras, M. Antonietta; Saba, A.
Journal of Heterocyclic Chemistry, 1994 , vol. 31, # 5 p. 1289 - 1292
反应条件
1: 84 percent / 3-chloroperbenzoic acid / CH2Cl2 / Ambient temperature 2: 2.) N,N'-dimethylcarbamoyl chloride / 1.) CH2Cl2, 5 min, r.t.; 2.) 7 d View Scheme
参考文献
Burstall
Journal of the Chemical Society, 1938 , p. 1662,1669
反应条件
NiII chloride hexahydrate; iodine; acetic acid; lithium chloride; zinc in N,N-dimethyl-formamide T=50 - 70°C; 6 h;
参考文献
Liao, Lian-Yan; Kong, Xing-Rui; Duan, Xin-Fang
Journal of Organic Chemistry, 2014 , vol. 79, # 2 p. 777 - 782
反应条件
benzoyl chloride in water Ambient temperature;
参考文献
Antonini, Ippolito; Claudi, Francesco; Cristalli, Gloria; Franchetti, Palmarisa; Grifantini, Mario; Martelli, Sante
Journal of Medicinal Chemistry, 1981 , vol. 24, # 10 p. 1181 - 1184
反应条件
1: [2,2']bipyridinyl With 3-chloro-benzenecarboperoxoic acid in dichloromethane T=20°C; 20 h; 2: trimethylsilyl cyanide With N,N-dimethylcarbamoyl chloride in dichloromethane T=20°C; 48 h;
参考文献
Colacio, Enrique; Perea-Buceta, Jesus E.; Mota, Antonio J.; Brechin, Euan K.; Prescimone, Alessandro; Haenninen, Mikko; Seppaelae, Petri; Sillanpaeae, Reijo
Chemical Communications, 2012 , vol. 48, # 6 p. 805 - 807
参考文献
Burstall
Journal of the Chemical Society, 1938 , p. 1662,1669
反应条件
1: copper-powder; biphenyl 2: bromine / 500 °C 3: biphenyl View Scheme
参考文献
Burstall
Journal of the Chemical Society, 1938 , p. 1662,1669
参考文献
Chen, Zhuqi; Ding, Fei; Hao, Feng; Guan, Ming; Bian, Zuqiang; Ding, Bei; Huang, Chunhui
New Journal of Chemistry, 2010 , vol. 34, # 3 p. 487 - 494
反应条件
sodium azide; ammonium chloride in N,N-dimethyl-formamide
T=100°C; 24 h;
参考文献
Chen, Zhuqi; Ding, Fei; Hao, Feng; Guan, Ming; Bian, Zuqiang; Ding, Bei; Huang, Chunhui
New Journal of Chemistry, 2010 , vol. 34, # 3 p. 487 - 494
