N-(氨基亚氨基甲基)苯磺胺合成路线 (共 12 条)
反应条件
hydrazine hydrate T=105°C;
参考文献
Brown, Thomas B.; Lowe, Philip R.; Schwalbe, Carl H.; Stevens, Malcolm F.G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2485 - 2490
参考文献
Ackermann
Hoppe-Seyler's Zeitschrift fuer Physiologische Chemie, 1906 , vol. 47, p. 366
参考文献
Clarke; Gillespie
Journal of the American Chemical Society, 1932 , vol. 54, p. 1964,1966
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Perrot
Bulletin de la Societe Chimique de France, 1946 , p. 554,557
反应条件
water und anschliessenden Behandeln mit Benzolsulfonylchlorid und wss.NaOH;
参考文献
Bengelsdorf
Journal of the American Chemical Society, 1953 , vol. 75, p. 3138
反应条件
hydrogenchloride T=130°C;
参考文献
Perrot
Bulletin de la Societe Chimique de France, 1946 , p. 554,557
反应条件
ammonia; phenol T=110°C;
参考文献
Gompper,R.; Haegele,W.
Chemische Berichte, 1966 , vol. 99, p. 2885 - 2899
参考文献
Am.Cyanamid Co.
Patent: US2359363 , 1942 ;
反应条件
1: 1.) NaNO2, 2M HCl, 2.) NaN3 / 1.) H2O, 0 deg C 2: 67 percent / hydrazine hydrate / 105 °C View Scheme
参考文献
Brown, Thomas B.; Lowe, Philip R.; Schwalbe, Carl H.; Stevens, Malcolm F.G.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2485 - 2490
反应条件
1: benzene / 110 °C 2: aqueous hydrochloric acid / 130 °C View Scheme
参考文献
Perrot
Bulletin de la Societe Chimique de France, 1946 , p. 554,557
反应条件
1: (i) aq. NaOH, (ii) MeHal 2: NH3, PhOH / 110 °C View Scheme
参考文献
Gompper,R.; Haegele,W.
Chemische Berichte, 1966 , vol. 99, p. 2885 - 2899