Geske, Grant D.; Wezeman, Rachel J.; Siegel, Adam P.; Blackwell, Helen E.
Journal of the American Chemical Society, 2005 , vol. 127, # 37 p. 12762 - 12763
Spandl, Richard J.; Nicholson, Rebecca L.; Marsden, David M.; Hodgkinson, James T.; Su, Xianbin; Thomas, Gemma L.; Salmond, George P. C.; Welch, Martin; Spring, David R.
Synlett, 2008 , # 14 p. 2122 - 2126
1: dimethyl malonate With n-butyllithium in diethyl ether
T=-78 - -10°C;
2: butyryl chloride in diethyl ether
T=-10°C; 0.5 h;
参考文献
Geske, Grant D.; Wezeman, Rachel J.; Siegel, Adam P.; Blackwell, Helen E.
Journal of the American Chemical Society, 2005 , vol. 127, # 37 p. 12762 - 12763
Spandl, Richard J.; Nicholson, Rebecca L.; Marsden, David M.; Hodgkinson, James T.; Su, Xianbin; Thomas, Gemma L.; Salmond, George P. C.; Welch, Martin; Spring, David R.
Synlett, 2008 , # 14 p. 2122 - 2126
