[(E)-2-苯基乙烯基]硼酸合成路线 （共 20 条）
反应条件
acetyl chloride T=25°C; 18 h;
参考文献
Tetrahedron Letters, , vol. 53, # 35 p. 4721 - 4724
反应条件
sodium carbonate; triphenylphosphine; palladium diacetate in toluene T=100°C; Suzuki cross-coupling; 12 h;
参考文献
Lim, Kyoung-Chan; Hong, Young-Taek; Kim, Sunggak
Synlett, 2006 , # 12 p. 1851 - 1854
反应条件
NH4I; Cu(NO3)2*3H2O; oxygen; acetic acid T=130°C; 18 h; optical yield given as percent de;
参考文献
Kim, Jinho; Choi, Jiho; Shin, Kwangmin; Chang, Sukbok
Journal of the American Chemical Society, 2012 , vol. 134, # 5 p. 2528 - 2531
反应条件
[{Rh(OH)(cod)}2]; potassium carbonate in 1,4-dioxane T=80°C; 4 h; Inert atmosphere;
参考文献
Anbarasan, Pazhamalai; Neumann, Helfried; Beller, Matthias
Angewandte Chemie - International Edition, 2011 , vol. 50, # 2 p. 519 - 522
反应条件
Ag2CO3; copper(II) bis(trifluoromethanesulfonate); potassium carbonate in N,N-dimethyl-formamide T=100°C; 20 h;
参考文献
Zhang, Guangyou; Chen, Shuyou; Fei, Haiyang; Cheng, Jiang; Chen, Fan
Synlett, 2012 , vol. 23, # 15 p. 2247 - 2250
反应条件
[Rh(acac)2(CO)2] in tetrahydrofuran; water T=70°C; 15 h; Inert atmosphere;
参考文献
Jana, Ranjan; Tunge, Jon A.
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8376 - 8385
反应条件
potassium carbonate in ethanol; water T=70°C; Suzuki-Miyaura reaction; 14 h;
参考文献
Chtchigrovsky, Melanie; Lin, Yi; Ouchaou, Kahina; Chaumontet, Manon; Robitzer, Mike; Quignard, Francoise; Taran, Frederic
Chemistry of Materials, 2012 , vol. 24, # 8 p. 1505 - 1510
反应条件
1: 2-Phenylvinylboronic With PPh3 gold(I) chloro complex; caesium carbonate in isopropyl alcohol T=50°C; Inert atmosphere; 2: para-iodobenzonitrile With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in acetonitrile Inert atmosphere;
参考文献
Hashmi, A. Stephen K.; Lothschuetz, Christian; Doepp, Rene; Rudolph, Matthias; Ramamurthi, Tanuja D.; Rominger, Frank
Angewandte Chemie - International Edition, 2009 , vol. 48, # 44 p. 8243 - 8246
反应条件
water in diethyl ether T=20°C; Inert atmosphere;
参考文献
Organic Letters, , vol. 16, # 2 p. 632 - 635
反应条件
1: Br2BH-SMe2; phenylacetylene in dichloromethane
T=0 - 20°C; Inert atmosphere;
2: water in diethyl ether; dichloromethane
T=0 - 20°C; Inert atmosphere;
参考文献
Gopula, Balraj; Chiang, Chien-Wei; Lee, Way-Zen; Kuo, Ting-Shen; Wu, Ping-Yu; Henschke, Julian P.; Wu, Hsyueh-Liang
Organic Letters, 2014 , vol. 16, # 2 p. 632 - 635
