2-溴甲基-1,3-二氧戊烷合成路线 (共 28 条)
反应条件
Dowex 50(H+) T=120°C; 1 h;
参考文献
Diaz-Ortiz; Diez-Barra; De La Hoz; Prieto
Synthetic Communications, 1993 , vol. 23, # 14 p. 1935 - 1942
反应条件
toluene-4-sulfonic acid T=110°C; 2 h;
参考文献
Conole, Grainne; Mears, Richard J.; Silva, Harshani De; Whiting, Andrew
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 14 p. 1825 - 1836
反应条件
bromine in tetrachloromethane T=60 - 70°C;
参考文献
Kotlyar; Pluzhnik-Gladyr'; Zlotskii
Russian Journal of General Chemistry, 1998 , vol. 68, # 2 p. 283 - 284
反应条件
bromine; di-tert-butyldicyclohexano-18-crown-18 in benzene T=20°C; Bromination; 0.166667 h;
参考文献
Kotlyar; Pluzhnik-Gladyr'
Russian Journal of General Chemistry, 1998 , vol. 68, # 6 p. 914 - 916
反应条件
sulfuric acid T=100°C;
参考文献
Hill; Pidgeon
Journal of the American Chemical Society, 1928 , vol. 50, p. 2723
参考文献
Hill; Pidgeon
Journal of the American Chemical Society, 1928 , vol. 50, p. 2723
Full Text Show Details
Hibbert; Hill
Journal of the American Chemical Society, 1923 , vol. 45, p. 747
参考文献
Hibbert; Perry; Taylor
Journal of the American Chemical Society, 1929 , vol. 51, p. 1554
参考文献
Gurwitsch
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 2888,2890; engl. Ausg. S. 2925
参考文献
Lee, Kheng H.; Brumby, Steven
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 1071 - 1074
反应条件
pyridine; N,N'-dimethyl-N,N'-propyleneurea; 1,10-phenanthroline; NiI2*3.5H2O; sodium iodide; zinc T=20 - 60°C; 19 h; chemoselective reaction;
参考文献
Everson, Daniel A.; Jones, Brittany A.; Weix, Daniel J.
Journal of the American Chemical Society, 2012 , vol. 134, # 14 p. 6146 - 6159