1-对茴香基-1-苯基乙烯合成路线 （共 99 条）
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=-78 - 20°C; 2 h; Inert atmosphere;
参考文献
Singh, Fateh V.; Milagre, Humberto M.S.; Eberlin, Marcos N.; Stefani, Helio A.
Tetrahedron Letters, 2009 , vol. 50, # 20 p. 2312 - 2316
反应条件
CaY zeolite in hexane 3 h; Ambient temperature; Yield givenYields of byproduct given;
参考文献
Kao, Hsien-Ming; Grey, Clare P.; Pitchumani, Kasi; Lakshminarasimhan; Ramamurthy
Journal of Physical Chemistry A, 1998 , vol. 102, # 28 p. 5627 - 5638
反应条件
1: With 2-Iodo-5-methylbenzenesulfonic acid in tert-butyl methyl ether; water; isopropyl alcohol T=22°C; 0.0833333 h; Inert atmosphere; 2: With Oxonereg; in tert-butyl methyl ether; water; isopropyl alcohol T=22°C; 46 h; Inert atmosphere; regioselective reaction; Further stages;
参考文献
Purohit, Vikram C.; Allwein, Shawn P.; Bakale, Roger P.
Organic Letters, 2013 , vol. 15, # 7 p. 1650 - 1653
反应条件
Behandlung des Jodhydrins mit Silbernitrat;
参考文献
Tiffeneau; Orechow
Bulletin de la Societe Chimique de France, 1925 , vol. <4>37, p. 437
反应条件
Behandeln des in Benzol geloesten Reaktionsprodukts mit Wasser und mit wss. Na2CO3;
参考文献
Bergmann et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1612,1614
反应条件
in cyclohexane Kinetics; Irradiation (UV/VIS); under N2, soln. of W(CO)5CPh2 in C6H12 added to soln. of alkene in C6H12, irradiated through Pyrex filter at 25.+-.1°C for 4 h / kinetics monitored at 12-14 and 27-29°C by UV; concd. in vac., extd. with cold pentane (-10°C), evapd., redissolved in CCl4, chromd. (SiO2/deactivated with H2O, CCl4, -15°C), collected at 0°C, evapd. in vac., dissolved in pentane, evapd. in vac.; elem. anal.;
参考文献
Fong,L.K.; Cooper,N.J.
Journal of the American Chemical Society, 1984 , vol. 106, p. 2595
反应条件
in cyclohexane under N2, soln. of W(CO)5CPh2 in C6H12 added to soln. of alkene in C6H12, heated at 30°C in the dark for 2 weeks; evapd. in vac., chromd. (SiO2);
参考文献
Journal of the American Chemical Society, , vol. 106, p. 2595
反应条件
in cyclohexane under N2, soln. of W(CO)5CPh2 in C6H12 added to soln. of alkene in C6H12, heated at 30°C in the dark for 2 weeks; evapd. in vac., chromd. (SiO2);
参考文献
Journal of the American Chemical Society, , vol. 106, p. 2595
反应条件
sodium acetate; Pd-montmorillonite in 1-methyl-pyrrolidin-2-one
T=150°C; Heck reaction; 2 h;
参考文献
Molnar, Arpad; Papp, Attila
Synlett, 2006 , # 18 p. 3130 - 3134
反应条件
sodium carbonate; Pd-montmorillonite in 1-methyl-pyrrolidin-2-one
T=150°C; Heck reaction; 6 h;
参考文献
Molnar, Arpad; Papp, Attila
Synlett, 2006 , # 18 p. 3130 - 3134
