1,1,2,3,3-五氟丙烯合成路线 (共 12 条)
反应条件
hydrogen
T=300 - 450°C; 0.002 - 0.003 h;
参考文献
Iikubo, Yuichi; Hedrick, Vicki; Brandstadter, Stephen M.; Cohn, Mitchel
Patent: US2004/127757 A1, 2004 ;
Location in patent: Page 5 ;
反应条件
hydrogen
T=100 - 135°C; 0.00845278 h;
参考文献
Iikubo, Yuichi; Hedrick, Vicki; Brandstadter, Stephen M.; Cohn, Mitchel
Patent: US2004/127757 A1, 2004 ;
Location in patent: Page 5 ;
反应条件
1,1,2,2-tetrafluoroethylene
T=150°C; 18 h; Further byproducts given;
参考文献
Haszeldine, Robert N.; Rowland, Ronald; Speight, James G.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 314 - 324
参考文献
Fainberg; Miller
Journal of the American Chemical Society, 1957 , vol. 79, p. 4170,4174
反应条件
T=150°C; 18 h; Further byproducts given;
参考文献
Haszeldine, Robert N.; Rowland, Ronald; Speight, James G.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 314 - 324
反应条件
T=200°C; 10 h; Further byproducts given;
参考文献
Haszeldine, Robert N.; Rowland, Ronald; Speight, James G.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 314 - 324
反应条件
T=200°C; 320 h; Further byproducts given;
参考文献
Haszeldine, Robert N.; Rowland, Ronald; Speight, James G.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 314 - 324
反应条件
hydrogenchloride; cadmium (II) iodide; cadmium
1) a) DMF, 0 deg C, 1h b) 1h, r.t.; Yield given. Multistep reaction;
参考文献
Burton, Donald J.; Tarumi, Yasuo; Heinze, Pamela L.
Journal of Fluorine Chemistry, 1990 , vol. 50, # 2 p. 257 - 263
反应条件
T=300°C; 160 h; Further byproducts given;
参考文献
Haszeldine, Robert N.; Rowland, Ronald; Speight, James G.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 314 - 324
反应条件
Pyrex tube
T=200°C; 320 h; further periods of contact time, other temperatures; Product distributionMechanism;
参考文献
Haszeldine, Robert N.; Rowland, Ronald; Speight, James G.; Tipping, Anthony E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 314 - 324