in neat (no solvent)
byproducts: C2F4, C3F6, SiF4; carried out under inert atm.; combined and heated to 170°C, detected after 3h to 80h, no longer detected after further 72h at 170°C; not isolated, monitored by NMR;
参考文献
Ganja, E. A.; Morrison, J. A.
Inorganic Chemistry, 1990 , vol. 29, p. 33 - 38
in neat (no solvent)
byproducts: CF3I; carried out in an inert atm., reactor loaded with educts and heated to 165°C; only trace amounts (0.2percent) detected by NMR;
参考文献
Ganja, E. A.; Morrison, J. A.
Inorganic Chemistry, 1990 , vol. 29, p. 33 - 38
Dale, J. V.; Emeleus, H. J.; Haszeldine, R. N.; Moss, J. H.
Journal of the Chemical Society, 1957 , p. 3708 - 3713
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Gmelin Handbook: F: PerFHalOrg.3, 3, page 226 - 232
