1-[(三甲基锡烷基)甲基]苯合成路线 (共 28 条)
反应条件
in dichloromethane 0 gradC for 2 h. then room temp. overnight;
参考文献
Yamaguchi, Ryohei; Moriyasu, Masataka; Kawanisi, Mituyosi
Tetrahedron Letters, 1986 , vol. 27, # 2 p. 211 - 214
反应条件
in dimethyl sulfoxide byproducts: toluene; alkaline decompn.; mechanism discussed;;
参考文献
Alexander, R.; Eaborn, C.; Traylor, T. G.
Journal of Organometallic Chemistry, 1970 , vol. 21, p. P65 - P66
反应条件
PdCl(COPh)(PPh3)2 in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=65°C; 12 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Labadie, Jeff W.; Tueting, David; Stille, J. K.
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4634 - 4642
反应条件
bis(η3-allyl-μ-chloropalladium(II)) in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=20°C; 0.166667 h; Mechanism;
参考文献
Bumagin, N. A.; Bumagina, I. G.; Kashin, A. N.; Beletskaya, I. P.
Journal of Organic Chemistry USSR (English Translation), 1982 , p. 977 - 981
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 6 p. 1131 - 1137
反应条件
ammonia in acetonitrile BzSnMe3 in CH3CN added to Fe(phen)3(PF6)3 in CH3CN at 22°C underAr and soln. stirred for 2 h, drop water added and Fe(II) complex filtered, filtrate dried with MgSO4 and treated anhyd. NH3 and Sn product filtered;
参考文献
Journal of the American Chemical Society, , vol. 104, # 5 p. 1319 - 1330
反应条件
sodium hydroxide 1.) 22 deg C; Yield given. Multistep reaction;
参考文献
Rollick; Kochi
Journal of the American Chemical Society, 1982 , vol. 104, # 5 p. 1319 - 1330
反应条件
aluminum tri-bromide in dichloromethane T=-50°C; 0.0833333 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 35, p. 1911 - 1915
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 2097 - 2101
反应条件
aluminum tri-bromide
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 35, p. 1911 - 1915
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 2097 - 2101
反应条件
iodine in methanol Kinetics; mixture was left in the dark overnight at 298 K; poured into water, extrd. (CCl4), dried (Na2SO4), NMR;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 89, # 10 p. 819 - 830
反应条件
bromine in not given byproducts: C6H5CH2Br;
参考文献
Boue, S.; Gielen, M.; Nasielski, J.
Journal of Organometallic Chemistry, 1967 , vol. 9, p. 461 - 479