tert.-butylhydroperoxide; 3 A molecular sieve in chloroform T=40°C; 72 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
1: 96.5 g / magnesium / tetrahydrofuran / Ambient temperature 2: 64 percent / Jones chromic acid reagent / acetone / 0 °C View Scheme
参考文献
Adams, David R.; Barnes, Alan F.; Cassidy, Frederick; Thompson, Mervyn
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2061 - 2068