1,2-二氯-1,1,3,3-五氟丙烷合成路线 (共 24 条)
参考文献
Honeywell International Inc.
Patent: US7473810 B1, 2009 ;
Location in patent: Page/Page column 8 ;
参考文献
McBee; Truchan; Bolt
Journal of the American Chemical Society, 1948 , vol. 70, p. 2023
反应条件
hydrogen fluoride
T=260°C; P=760.051 Torr; 0.00833333 h; Gas phase; Product distribution / selectivity;
参考文献
E.I. DUPONT DE NEMOURS AND COMPANY
Patent: WO2005/37744 A1, 2005 ;
Location in patent: Page/Page column 13-14; 15 ;
反应条件
hydrogen fluoride; catalyst from preparation example 1 (99percent Cr/1percent Cu)
T=280 - 320°C; P=760.051 Torr; 0.00138889 h; Gas phase; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2007/19357 A1, 2007 ;
Location in patent: Page/Page column 12-14 ;
反应条件
hydrogen fluoride; Cr(NO3)3/ZnCl2 98.1/1.9 calcined at 550 C
T=300 - 350°C; P=760.051 Torr; 0.00416667 h; Gas phase; Product distribution / selectivity;
参考文献
E.I. DUPONT DE NEMOURS AND COMPANY
Patent: WO2005/37744 A1, 2005 ;
Location in patent: Page/Page column 13-14; 15 ;
反应条件
chlorine
T=2 - 3°C; 3 h; Irradiation;
参考文献
E.I. DUPONT DE NEMOURS AND COMPANY
Patent: WO2006/69105 A1, 2006 ;
Location in patent: Page/Page column 12 ;
反应条件
hydrogen fluoride; catalyst from preparation example 4 (98percent Cr/2percent Cu)
T=280 - 320°C; P=760.051 Torr; 0.00138889 h; Gas phase; Product distribution / selectivity;
参考文献
E. I. DU PONT DE NEMOURS AND COMPANY
Patent: WO2007/19357 A1, 2007 ;
Location in patent: Page/Page column 12-14 ;
反应条件
chlorine
T=20°C; 0.00472222 h; Irradiation;
参考文献
E.I. DUPONT DE NEMOURS AND COMPANY
Patent: WO2006/69105 A1, 2006 ;
Location in patent: Page/Page column 13 ;
反应条件
hydrogen fluoride; Cr(NO3)3[9(H2O)]; AgNO3; calcined
T=300 - 400°C; 0.00416667 - 0.00494444 h; Product distribution / selectivity;
参考文献
Rao, Velliyur Nott Mallikarjuna; Sievert, Allen Capron
Patent: US2008/207963 A1, 2008 ;
Location in patent: Page/Page column 8-9 ;
反应条件
hydrogen fluoride; antimony(V) pentachloride
T=250°C; unter Druck;
参考文献
McBee; Truchan; Bolt
Journal of the American Chemical Society, 1948 , vol. 70, p. 2023