3-碘季戊四醇氟代丙烷-1合成路线 （共 17 条）
反应条件
N,N-dimethyl-formamide; potassium iodide in acetonitrile T=0°C; 3.21667 h;
参考文献
Wlassics, Ivan; Tortelli, Vito; Carella, Serena; Monzani, Cristiano; Marchionni, Giuseppe
Molecules, 2011 , vol. 16, # 8 p. 6512 - 6540
反应条件
potassium iodide in diethylene glycol dimethyl ether T=0 - 25°C; 1 h;
参考文献
Petrov, V. A.
Journal of Fluorine Chemistry, 1995 , vol. 73, # 1 p. 17 - 20
反应条件
acetone; sodium iodide
参考文献
Miller et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 4159,4163
参考文献
Fainberg; Miller
Journal of the American Chemical Society, 1957 , vol. 79, p. 4170,4174
参考文献
Fainberg; Miller
Journal of the American Chemical Society, 1957 , vol. 79, p. 4170,4174
反应条件
zinc in N,N-dimethyl-formamide
参考文献
Burton, Donald J.; Tarumi, Yasuo; Heinze, Pamela L.
Journal of Fluorine Chemistry, 1990 , vol. 50, # 2 p. 257 - 263
参考文献
Fainberg; Miller
Journal of the American Chemical Society, 1957 , vol. 79, p. 4170,4174
反应条件
1,4-dioxane; potassium hydroxide
参考文献
Knunjanz; Djatkin
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1958 , p. 648; engl. Ausg. S. 633
反应条件
nitrogen(II) oxide; mercury
Irradiation;
参考文献
Tarrant,P.; Savory,J.
Journal of Organic Chemistry, 1963 , vol. 28, p. 1728 - 1730
→
83168-66-5(2Z,4E)-1,1,1,2,3,4,5,6,6,6-十氟己-2,4-二烯+ 83168-67-6(2E,4E)-1,1,1,2,3,4,5,6,6,6-十氟己-2,4-二烯+ 83168-65-4(2Z,4Z)-1,1,1,2,3,4,5,6,6,6-十氟己-2,4-二烯
反应条件
tetracarbonylnickel(0) in acetonitrile
Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Krespan, Carl G.; Dixon, David A.
Journal of Organic Chemistry, 1998 , vol. 63, # 1 p. 36 - 43
