(S)-(+)-1,2-丙二醇合成路线 (共 56 条)
参考文献
Neuberg; Vercellone
Biochemische Zeitschrift, 1935 , vol. 279, p. 140
反应条件
pyridine in dichloromethane T=-25 - 20°C; 8 h; Inert atmosphere;
参考文献
Turgut, Yilmaz; Aral, Tarik; Hosgoren, Halil
Tetrahedron Asymmetry, 2009 , vol. 20, # 19 p. 2293 - 2298
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Turgut, Yilmaz; Aral, Tarik; Karakaplan, Mehmet; Deniz, Pinar; Hosgoren, Halil
Synthetic Communications, 2010 , vol. 40, # 22 p. 3365 - 3377
反应条件
triphenylphosphine in tetrachloromethane 4 h; Heating;
参考文献
Tsuboi, Sadao; Kohara, Noriyuki; Doi, Katsumi; Utaka, Masanori; Takeda, Akira
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 3205 - 3210
反应条件
triethylamine in dichloromethane T=20°C; Inert atmosphereCooling with ice;
参考文献
Kuriyama, Wataru; Ino, Yasunori; Ogata, Osamu; Sayo, Noboru; Saito, Takao
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 1 p. 92 - 96
反应条件
Yield given. Multistep reaction;
参考文献
Sugawara, Fumio; Nakayama, Haruhiko; Ogawa, Tomoya
Carbohydrate Research, 1983 , vol. 123, p. C25 - C28
反应条件
4-(N,N-dimethlyamino)pyridine; potassium hydroxide; triethylamine in dichloromethane
反应条件
tetrabutylammomium bromide; bis(tri-n-butyltin)oxide in benzene 16 h; Heating;
参考文献
Agricultural and Biological Chemistry, , vol. 50, # 9 p. 2261 - 2272
反应条件
4-(N,N-dimethlyamino)pyridine; potassium hydroxide; triethylamine in dichloromethane
反应条件
tetrabutylammomium bromide; bis(tri-n-butyltin)oxide in benzene 16 h; Heating;
参考文献
Agricultural and Biological Chemistry, , vol. 50, # 9 p. 2261 - 2272
反应条件
potassium carbonate; triphenylphosphine in tetrachloromethane 24 h; Heatingvar. cyclodehydr. reag., var. solv., var. temp.; regioselectivity; Product distribution;
参考文献
Robinson, Philip L.; Barry, Carey N.; Bass, S. Woody; Jarvis, Susan E.; Evans, Slayton A.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5396 - 5398