甲基3,5-二碘-4-甲氧基苯甲酸酯合成路线 (共 12 条)
反应条件
sodium tetrahydroborate; sodium ditelluride in ethanol 4 h; Heating; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 63, # 12 p. 3911 - 3917
反应条件
sodium selenide; sodium tetrahydroborate 4 h; Heating; Yield given. Yields of byproduct given;
参考文献
Vasil'ev, Andrei A.; Engman, Lars
Journal of Organic Chemistry, 1998 , vol. 63, # 12 p. 3911 - 3917
反应条件
sodium hydrogen telluride; acetic acid in ethanol 4 h; Heating; Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 63, # 12 p. 3911 - 3917
反应条件
sodium selenide; sodium tetrahydroborate 4 h; Heating; Yield given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 63, # 12 p. 3911 - 3917
反应条件
sodium tetrahydroborate; sodium ditelluride in ethanol 4 h; Heating; Yield given. Yields of byproduct given;
参考文献
Vasil'ev, Andrei A.; Engman, Lars
Journal of Organic Chemistry, 1998 , vol. 63, # 12 p. 3911 - 3917
反应条件
hydrazine hydrate in methanol 2 h; Inert atmosphereReflux;
参考文献
Grimster, Neil P.; Connelly, Stephen; Baranczak, Aleksandra; Dong, Jiajia; Krasnova, Larissa B.; Sharpless, K. Barry; Powers, Evan T.; Wilson, Ian A.; Kelly, Jeffery W.
Journal of the American Chemical Society, 2013 , vol. 135, # 15 p. 5656 - 5668
反应条件
sodium hydrogen telluride; acetic acid in ethanol 4 h; Heating; Yields of byproduct given;
参考文献
Vasil'ev, Andrei A.; Engman, Lars
Journal of Organic Chemistry, 1998 , vol. 63, # 12 p. 3911 - 3917
反应条件
potassium carbonate in acetone
16 h; Heating;
参考文献
Zhou, Qin; Swager, Timothy M.
Journal of the American Chemical Society, 1995 , vol. 117, # 50 p. 12593 - 12602
反应条件
1: 4-hydroxy-3,5-diiodobenzoic acid With potassium carbonate in N,N-dimethyl-formamide
T=20°C; Inert atmosphere;
2: methyl iodide in N,N-dimethyl-formamide
T=20°C; Inert atmosphere;
参考文献
Grimster, Neil P.; Connelly, Stephen; Baranczak, Aleksandra; Dong, Jiajia; Krasnova, Larissa B.; Sharpless, K. Barry; Powers, Evan T.; Wilson, Ian A.; Kelly, Jeffery W.
Journal of the American Chemical Society, 2013 , vol. 135, # 15 p. 5656 - 5668
反应条件
1: 92 percent / H2SO4 / Heating
2: 90 percent / K2CO3 / acetone / 16 h / Heating
View Scheme
参考文献
Zhou, Qin; Swager, Timothy M.
Journal of the American Chemical Society, 1995 , vol. 117, # 50 p. 12593 - 12602