in dichloromethane Irradiation (UV/VIS); addn. of soln. of radical precursor to soln. of Co-compd. in CH2Cl2 at 0°C (under N2) with stirring, illumination with a 500 W sunlamp for 12 h; bringing to room temp., concn. the volume, chromy. (silica gel, eluent: pentane and CH2Cl2 for organic products, CH2Cl2/ethyl acetate for inorganic product), elem. anal.;
参考文献
Das, Indira; Roy, Sujit
Journal of Organometallic Chemistry, 1994 , vol. 464, # 2 p. 233 - 238
Truchet
Annales de Chimie (Cachan, France), 1931 , vol. <10>16, p. 396
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1930 , vol. 191, p. 855
