N-叔丁基-4-甲基苯甲酰胺合成路线 (共 18 条)
反应条件
sodium hydroxide; potassium chloride; water T=100°C; hydrolysis and oxygen exchange rate constants; Rate constant;
参考文献
Slebocka-Tilk; Bennet; Keillor; Brown; Guthrie, J. Peter; Jodhan
Journal of the American Chemical Society, 1990 , vol. 112, # 23 p. 8507 - 8514
参考文献
Bayer Aktiengesellschaft
Patent: US4496736 A1, 1985 ;
反应条件
sodium hydroxide; potassium chloride; water T=100°C; hydrolysis and oxygen exchange rate constants; Rate constant;
参考文献
Slebocka-Tilk; Bennet; Keillor; Brown; Guthrie, J. Peter; Jodhan
Journal of the American Chemical Society, 1990 , vol. 112, # 23 p. 8507 - 8514
参考文献
Centaur Pharmaceuticals, Inc.
Patent: US5472983 A1, 1995 ;
反应条件
sulfuric acid
T=42°C; 2 h;
参考文献
Reddy, K. Laxma
Tetrahedron Letters, 2003 , vol. 44, # 7 p. 1453 - 1455
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=90°C;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031
反应条件
alum in neat (no solvent)
T=100°C; Ritter Amidation; 1.5 h;
参考文献
Sadeghi, Bahareh; Farahzadi, Ebrahim; Hassanabadi, Alireza
Journal of Chemical Research, 2012 , vol. 36, # 9 p. 539 - 540
反应条件
sodium carbonate; trans-di(μ-acetato)bis[o-(di-o-tolylphosphino)benzyl]dipalladium(II) in water
T=170°C; 0.166667 h; microwave irradiation;
参考文献
Wu, Xiongyu; Larhed, Mats
Organic Letters, 2005 , vol. 7, # 15 p. 3327 - 3329
参考文献
Sumitomo Pharmaceuticals Company, Limited
Patent: US6384033 B1, 2002 ;
反应条件
water; triphenylphosphine; cesium fluoride; palladium dichloride in dimethyl sulfoxide
T=110°C; 15 h;
参考文献
Jiang, Huanfeng; Liu, Bifu; Li, Yibiao; Wang, Azhong; Huang, Huawen
Organic Letters, 2011 , vol. 13, # 5 p. 1028 - 1031